5-ethyl-2,2-dimethyl-[1,3]-dioxane-5-carboxylic acid benzyloxycarbonylmethyl ester

Base Information

Chemical Name:5-ethyl-2,2-dimethyl-[1,3]-dioxane-5-carboxylic acid benzyloxycarbonylmethyl ester
CAS No.:1609647-70-2
Molecular Formula:C₁₈H₂₄O₆
Molecular Weight:336.385
Hs Code.:

Synonyms:5-ethyl-2,2-dimethyl-[1,3]-dioxane-5-carboxylic acid benzyloxycarbonylmethyl ester

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Chemical Property of 5-ethyl-2,2-dimethyl-[1,3]-dioxane-5-carboxylic acid benzyloxycarbonylmethyl ester

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Technology Process of 5-ethyl-2,2-dimethyl-[1,3]-dioxane-5-carboxylic acid benzyloxycarbonylmethyl ester

There total 2 articles about 5-ethyl-2,2-dimethyl-[1,3]-dioxane-5-carboxylic acid benzyloxycarbonylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 140-18-1
Benzyl chloroacetate

: 587874-07-5
5-ethyl-2,2-dimethyl-[1,3]-dioxane-5-carboxylic acid

: 1609647-70-2
5-ethyl-2,2-dimethyl-[1,3]-dioxane-5-carboxylic acid benzyloxycarbonylmethyl ester

Guidance literature:: With triethylamine; In 1-methyl-pyrrolidin-2-one; at 0 - 20 ℃;

Reference yield:

: 10097-02-6
2,2-bis(hydroxymethyl)butanoic acid

: 1609647-70-2
5-ethyl-2,2-dimethyl-[1,3]-dioxane-5-carboxylic acid benzyloxycarbonylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / toluene / 5 h / 80 °C

2: triethylamine / 1-methyl-pyrrolidin-2-one / 0 - 20 °C

With pyridinium p-toluenesulfonate; triethylamine; In 1-methyl-pyrrolidin-2-one; toluene;