5-(2-hydroxy-3-methoxybenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione

Base Information

Chemical Name:5-(2-hydroxy-3-methoxybenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione
CAS No.:860725-77-5
Molecular Formula:C₁₄H₁₄N₂O₅
Molecular Weight:290.276
Hs Code.:

Synonyms:5-(2-hydroxy-3-methoxybenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione

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Chemical Property of 5-(2-hydroxy-3-methoxybenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione

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Technology Process of 5-(2-hydroxy-3-methoxybenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione

There total 1 articles about 5-(2-hydroxy-3-methoxybenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 769-42-6
1,3-dimethylbarbituric acid

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 860725-77-5
5-(2-hydroxy-3-methoxybenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione

Guidance literature:: In water; at 100 ℃; for 0.5h;
DOI:10.2174/157340611795564231

Reference yield:

: 40018-26-6
1,4-dithiane-2,5-diol

: 860725-77-5
5-(2-hydroxy-3-methoxybenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione

: 4-hydroxy-1-(2-hydroxy-3-methoxyphenyl)-7,9-dimethyl-2-thia-7,9-diazaspiro[4.5]decane-6,8,10-trione

Guidance literature:: In water; at 50 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2017.06.029

Reference yield:

: 860725-77-5
5-(2-hydroxy-3-methoxybenzylidene)-1,3-dimethyl-2,4,6(1H,3H,5H)pyrimidinetrione

: 4055-17-8
5-isopropenyl-2,3-dihydrothiophene 1,1-dioxide

: 1185843-41-7
(5R)-5-(2-hydroxy-3-methoxyphenyl)-1',3',7-trimethyl-3,3a,5,6-tetrahydro-2H,2'H-spiro[1-benzothiophene-4,5'-pyrimidine]-2',4',6'(1'H,3'H)-trione 1,1-dioxide

: 1185843-42-8
(5S)-5-(2-hydroxy-3-methoxyphenyl)-1',3',7-trimethyl-3,3a,5,6-tetrahydro-2H,2'H-spiro[1-benzothiophene-4,5'-pyrimidine]-2',4',6'(1'H,3'H)-trione 1,1-dioxide

Guidance literature:: With zinc(II) bis(L-proline); In 1,4-dioxane; water; for 20 - 38h; optical yield given as %de; Reflux;
DOI:10.1134/S1070428009010126