2-CARBOETHOXYPHENYL CYCLOHEXYL KETONE

Base Information

• Chemical Name: 2-CARBOETHOXYPHENYL CYCLOHEXYL KETONE
• CAS No.: 898792-17-1
• Molecular Formula: C₁₆H₂₀O₃
• Molecular Weight: 260.333
• Mol file: 898792-17-1.mol

Synonyms:ethyl 2-(cyclohexanecarbonyl)benzoate

Chemical Property of 2-CARBOETHOXYPHENYL CYCLOHEXYL KETONE

Chemical Property:

• Vapor Pressure: 2.57E-06mmHg at 25°C

Purity/Quality:

95% ^*data from raw suppliers

2-Carboethoxyphenylcyclohexylketone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-CARBOETHOXYPHENYL CYCLOHEXYL KETONE

There total 2 articles about 2-CARBOETHOXYPHENYL CYCLOHEXYL KETONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

cyclohexanylcarbonyl chloride (2719-27-9) + (2-(ethoxycarbonyl)phenyl)zinc(II) bromide → ethyl 2-(cyclohexanecarbonyl)benzoate (898792-17-1)

Guidance literature:

With bis(acetylacetonate)nickel(II); In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1016/j.tetlet.2011.01.135

Reference yield: 69.0%

ethyl 2-iodobenzoate (1829-28-3) + cyclohexanecarbaldehyde (2043-61-0) → ethyl 2-(cyclohexanecarbonyl)benzoate (898792-17-1)

Guidance literature:

With tert.-butylhydroperoxide; palladium diacetate; silver(l) oxide; In water; at 120 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.joc.6b01064

upstream raw materials:

cyclohexanylcarbonyl chloride

ethyl 2-iodobenzoate

cyclohexanecarbaldehyde