tert-butyl(((2S,4S)-5-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl)oxy)diphenylsilane

Base Information

Chemical Name:tert-butyl(((2S,4S)-5-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl)oxy)diphenylsilane
CAS No.:1297531-62-4
Molecular Formula:C₃₁H₄₂O₃Si
Molecular Weight:490.758
Hs Code.:

Synonyms:tert-butyl(((2S,4S)-5-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl)oxy)diphenylsilane

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Chemical Property of tert-butyl(((2S,4S)-5-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl)oxy)diphenylsilane

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Technology Process of tert-butyl(((2S,4S)-5-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl)oxy)diphenylsilane

There total 5 articles about tert-butyl(((2S,4S)-5-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl)oxy)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 89238-99-3
O-(4-methoxybenzyl)-trichloroacetimidate

: 638188-59-7
(2S,4S)-5-((tert-butyldiphenylsilyl)oxy)-2,4-dimethylpentan-1-ol

: 1297531-62-4
tert-butyl(((2S,4S)-5-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl)oxy)diphenylsilane

Guidance literature:: With CSA; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/ol200834p

Reference yield:

: 1297531-60-2
(S)-3-((S,E)-5-((tert-butyldiphenylsilyl)oxy)-4-methylpent-2-enoyl)-isopropyloxazolidin-2-one

: 1297531-62-4
tert-butyl(((2S,4S)-5-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl)oxy)diphenylsilane

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 24 h

2: lithium hexamethyldisilazane / tetrahydrofuran / 6.17 h / -78 - 0 °C / Inert atmosphere

3: lithium borohydride / tetrahydrofuran; water / 6 h / 0 °C

4: CSA / dichloromethane / 24 h / 20 °C

With lithium borohydride; palladium 10% on activated carbon; hydrogen; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; ethyl acetate;
DOI:10.1021/ol200834p

Reference yield:

: 1297531-61-3
(S)-3-((2S,4S)-5-((tert-butyldiphenylsilyl)oxy)-2,4-dimethylpentanoyl)-4-isopropyloxazolidin-2-one

: 1297531-62-4
tert-butyl(((2S,4S)-5-((4-methoxybenzyl)oxy)-2,4-dimethylpentyl)oxy)diphenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: lithium borohydride / tetrahydrofuran; water / 6 h / 0 °C

2: CSA / dichloromethane / 24 h / 20 °C

With lithium borohydride; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol200834p