6,7-dimethylbenz-2,3-dithiin

Base Information

Chemical Name:6,7-dimethylbenz-2,3-dithiin
CAS No.:37735-72-1
Molecular Formula:C₁₀H₁₂S₂
Molecular Weight:196.337
Hs Code.:

Synonyms:6,7-dimethylbenz-2,3-dithiin

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Chemical Property of 6,7-dimethylbenz-2,3-dithiin

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 6,7-dimethylbenz-2,3-dithiin

There total 5 articles about 6,7-dimethylbenz-2,3-dithiin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 114935-68-1
3,3,3-trimethyl-7,8-dimethylbenzo-2,4,3-dithiastibepin

: 4756-75-6
triphenyl antimony oxide

: 37735-72-1
6,7-dimethylbenz-2,3-dithiin

Guidance literature:: In neat (no solvent); crystn. of dithiin at about 25°C; recrystn. of dithhin from hexane (m.p.); identification of stibine oxide by m.p., elem. anal., IR;
DOI:10.1007/BF00956679

Reference yield: 25.0%

: 114935-67-0
3,3,3-triphenyl-7,8-dimethylbenzo-2,4,3-dithiastibepin

: 4756-75-6
triphenyl antimony oxide

: 37735-72-1
6,7-dimethylbenz-2,3-dithiin

Guidance literature:: In melt; melting in a sealed tube; extraction with ether, removal of solvent, isolation of disulfide by fractionated recrystn. from hexane, elem. anal., identification of triphenylstibine oxide by m.p., elem. anal. and IR;
DOI:10.1007/BF00956679

Reference yield: 23.0%

: 114935-67-0
3,3,3-triphenyl-7,8-dimethylbenzo-2,4,3-dithiastibepin

: 594-31-0,34716-91-1,20265-29-6
triphenylantimony dichloride

: 37735-72-1
6,7-dimethylbenz-2,3-dithiin

Guidance literature:: With chlorine; In benzene; refluxing for 1h; removal of solvent, isolation of disulfide, m.p.; isolation of Ph3SbCl2 by passing Cl2 through a soln. of Ph3Sb (m.p.);
DOI:10.1007/BF00956679