(5aRS,11bRS)-3,5a,6,11b-tetrahydro-1,5,5-trimethyl-3-phenyl-5H-<1>benzopyrano<3',4':4,5>pyrano<2,3-c>pyrazole

Base Information

Chemical Name:(5aRS,11bRS)-3,5a,6,11b-tetrahydro-1,5,5-trimethyl-3-phenyl-5H-<1>benzopyrano<3',4':4,5>pyrano<2,3-c>pyrazole
CAS No.:112296-62-5
Molecular Formula:C₂₂H₂₂N₂O₂
Molecular Weight:346.429
Hs Code.:

Synonyms:(5aRS,11bRS)-3,5a,6,11b-tetrahydro-1,5,5-trimethyl-3-phenyl-5H-<1>benzopyrano<3',4':4,5>pyrano<2,3-c>pyrazole

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Chemical Property of (5aRS,11bRS)-3,5a,6,11b-tetrahydro-1,5,5-trimethyl-3-phenyl-5H-<1>benzopyrano<3',4':4,5>pyrano<2,3-c>pyrazole

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Technology Process of (5aRS,11bRS)-3,5a,6,11b-tetrahydro-1,5,5-trimethyl-3-phenyl-5H-<1>benzopyrano<3',4':4,5>pyrano<2,3-c>pyrazole

There total 8 articles about (5aRS,11bRS)-3,5a,6,11b-tetrahydro-1,5,5-trimethyl-3-phenyl-5H-<1>benzopyrano<3',4':4,5>pyrano<2,3-c>pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 56074-73-8
2-(3-methyl-2-butenyloxy)benzaldehyde

: 89-25-8
edaravone

: 112296-62-5
(5aRS,11bRS)-3,5a,6,11b-tetrahydro-1,5,5-trimethyl-3-phenyl-5H-<1>benzopyrano<3',4':4,5>pyrano<2,3-c>pyrazole

Guidance literature:: With ethylenediamine diacetic acid; In acetonitrile; at 80 ℃; for 16h;
DOI:10.1021/jo00384a059

Reference yield:

: 56074-73-8
2-(3-methyl-2-butenyloxy)benzaldehyde

: 112296-62-5
(5aRS,11bRS)-3,5a,6,11b-tetrahydro-1,5,5-trimethyl-3-phenyl-5H-<1>benzopyrano<3',4':4,5>pyrano<2,3-c>pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / ethylenediammonium diacetate / acetonitrile / 18 h / Ambient temperature

2: ethylenediammonium diacetate / acetonitrile / 18 h / Heating

With ethylenediamine diacetic acid; In acetonitrile;
DOI:10.1021/jo00239a024

Reference yield:

: 89-25-8
edaravone

: 112296-62-5
(5aRS,11bRS)-3,5a,6,11b-tetrahydro-1,5,5-trimethyl-3-phenyl-5H-<1>benzopyrano<3',4':4,5>pyrano<2,3-c>pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / ethylenediammonium diacetate / acetonitrile / 18 h / Ambient temperature

2: ethylenediammonium diacetate / acetonitrile / 18 h / Heating

With ethylenediamine diacetic acid; In acetonitrile;
DOI:10.1021/jo00239a024