Z-β-chloroacrylic acid p-nitrophenyl ester

Base Information

• Chemical Name: Z-β-chloroacrylic acid p-nitrophenyl ester
• CAS No.: 35227-59-9
• Molecular Formula: C₉H₆ClNO₄
• Molecular Weight: 227.604
• Mol file: 35227-59-9.mol

Synonyms:Z-β-chloroacrylic acid p-nitrophenyl ester

Chemical Property of Z-β-chloroacrylic acid p-nitrophenyl ester

Chemical Property:

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Technology Process of Z-β-chloroacrylic acid p-nitrophenyl ester

There total 2 articles about Z-β-chloroacrylic acid p-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 3-chloroacrylic acid (1609-93-4) → Z-β-chloroacrylic acid p-nitrophenyl ester (35227-59-9)

Guidance literature:

With dmap; WSC*HCl; In dichloromethane; ethyl acetate; at 20 ℃; for 15h;

DOI:10.1021/ol0255965

Reference yield:

→ Z-β-chloroacrylic acid p-nitrophenyl ester (35227-59-9)

Guidance literature:

Cl-CH=CH-COOH, p-Nitrophenol, Benzol, P2O5 (70-80grad, 7 h);

upstream raw materials:

4-nitro-phenol

3-chloroacrylic acid