C₈H₅BrN₂S₂

Base Information

• Chemical Name: C₈H₅BrN₂S₂
• CAS No.: 1021953-80-9
• Molecular Formula: C₈H₅BrN₂S₂
• Molecular Weight: 273.177
• Mol file: 1021953-80-9.mol

Synonyms:C₈H₅BrN₂S₂

Chemical Property of C₈H₅BrN₂S₂

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₈H₅BrN₂S₂

There total 1 articles about C₈H₅BrN₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 4-bromobenzoic acid hydrazide (5933-32-4) → C8H5BrN2S2 (1021953-80-9)

Guidance literature:

carbon disulfide; 4-bromobenzoic acid hydrazide; With potassium hydroxide; In ethanol;

With hydrogenchloride;

DOI:10.1007/s11164-021-04510-x

Reference yield: 80.0%

iodobenzene (591-50-4) + C8H5BrN2S2 (1021953-80-9) → 2-(4-bromophenyl)-5-(phenylthio)-1,3,4-thiadiazole (1298111-49-5)

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 10h; regioselective reaction;

DOI:10.1016/j.tet.2011.02.064

Reference yield: 71.6%

C8H5BrN2S2 (1021953-80-9) + Nopyl-chlorid (13550-62-4) → 2-((2-(6,6-dimethylbicyclo[3.1.1]hept-2-en-2-yl)ethyl)thio)-5-(4-bromophenyl)-1,3,4-thiadiazole

Guidance literature:

With potassium carbonate; In acetone; for 6h; Reflux;

DOI:10.1007/s11164-021-04510-x

upstream raw materials:

carbon disulfide

4-bromobenzoic acid hydrazide

Downstream raw materials:

2-(4-bromophenyl)-5-(phenylthio)-1,3,4-thiadiazole