[(5-amino-1H-[1,2,4]triazol-3-yl)-(3,5-dichlorophenyl)amino]acetonitrile

Base Information

Chemical Name:[(5-amino-1H-[1,2,4]triazol-3-yl)-(3,5-dichlorophenyl)amino]acetonitrile
CAS No.:1533424-19-9
Molecular Formula:C₁₀H₈Cl₂N₆
Molecular Weight:283.12
Hs Code.:

Synonyms:[(5-amino-1H-[1,2,4]triazol-3-yl)-(3,5-dichlorophenyl)amino]acetonitrile

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Chemical Property of [(5-amino-1H-[1,2,4]triazol-3-yl)-(3,5-dichlorophenyl)amino]acetonitrile

Chemical Property:

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Technology Process of [(5-amino-1H-[1,2,4]triazol-3-yl)-(3,5-dichlorophenyl)amino]acetonitrile

There total 3 articles about [(5-amino-1H-[1,2,4]triazol-3-yl)-(3,5-dichlorophenyl)amino]acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1533424-99-5
(Z)-methyl N'-cyano-N-(cyanomethyl)-N-(3,5-dichlorophenyl)carbamimidothioate

: 1533424-19-9
[(5-amino-1H-[1,2,4]triazol-3-yl)-(3,5-dichlorophenyl)amino]acetonitrile

Guidance literature:: With hydrazine; In ethanol; at 65 ℃; under 760.051 Torr; Inert atmosphere;

Reference yield:

: 1533434-86-4
(Z)-methyl N'-cyano-N-(3,5-dichlorophenyl)carbamimidothioate

: 1533424-19-9
[(5-amino-1H-[1,2,4]triazol-3-yl)-(3,5-dichlorophenyl)amino]acetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C / 760.05 Torr / Inert atmosphere

1.2: 0 - 20 °C / 760.05 Torr / Inert atmosphere

2.1: hydrazine / ethanol / 65 °C / 760.05 Torr / Inert atmosphere

With sodium hydride; hydrazine; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 6590-93-8
3,5-dichlorophenylisothiocyanate

: 1533424-19-9
[(5-amino-1H-[1,2,4]triazol-3-yl)-(3,5-dichlorophenyl)amino]acetonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / methanol / 0.25 h / 760.05 Torr / Inert atmosphere

1.2: 1 h / 760.05 Torr / Inert atmosphere

1.3: 20 °C / 760.05 Torr / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C / 760.05 Torr / Inert atmosphere

2.2: 0 - 20 °C / 760.05 Torr / Inert atmosphere

3.1: hydrazine / ethanol / 65 °C / 760.05 Torr / Inert atmosphere

With sodium methylate; sodium hydride; hydrazine; In methanol; ethanol; N,N-dimethyl-formamide;