(Z)-methyl N'-cyano-N-(cyanomethyl)-N-(3,5-dichlorophenyl)carbamimidothioate

Base Information

Chemical Name:(Z)-methyl N'-cyano-N-(cyanomethyl)-N-(3,5-dichlorophenyl)carbamimidothioate
CAS No.:1533424-99-5
Molecular Formula:C₁₁H₈Cl₂N₄S
Molecular Weight:299.183
Hs Code.:

Synonyms:(Z)-methyl N'-cyano-N-(cyanomethyl)-N-(3,5-dichlorophenyl)carbamimidothioate

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Chemical Property of (Z)-methyl N'-cyano-N-(cyanomethyl)-N-(3,5-dichlorophenyl)carbamimidothioate

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Technology Process of (Z)-methyl N'-cyano-N-(cyanomethyl)-N-(3,5-dichlorophenyl)carbamimidothioate

There total 2 articles about (Z)-methyl N'-cyano-N-(cyanomethyl)-N-(3,5-dichlorophenyl)carbamimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 1533434-86-4
(Z)-methyl N'-cyano-N-(3,5-dichlorophenyl)carbamimidothioate

: 590-17-0
cyanomethyl bromide

: 1533424-99-5
(Z)-methyl N'-cyano-N-(cyanomethyl)-N-(3,5-dichlorophenyl)carbamimidothioate

Guidance literature:: (Z)-methyl N'-cyano-N-(3,5-dichlorophenyl)carbamimidothioate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h; under 760.051 Torr; Inert atmosphere;

cyanomethyl bromide; In N,N-dimethyl-formamide; at 0 - 20 ℃; under 760.051 Torr; Inert atmosphere;

Reference yield:

: 6590-93-8
3,5-dichlorophenylisothiocyanate

: 1533424-99-5
(Z)-methyl N'-cyano-N-(cyanomethyl)-N-(3,5-dichlorophenyl)carbamimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 0.25 h / 760.05 Torr / Inert atmosphere

1.2: 1 h / 760.05 Torr / Inert atmosphere

1.3: 20 °C / 760.05 Torr / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C / 760.05 Torr / Inert atmosphere

2.2: 0 - 20 °C / 760.05 Torr / Inert atmosphere

With sodium methylate; sodium hydride; In methanol; N,N-dimethyl-formamide;