C₄₁H₆₄F₂N₄O₄

Base Information

Chemical Name:C₄₁H₆₄F₂N₄O₄
CAS No.:1271776-74-9
Molecular Formula:C₄₁H₆₄F₂N₄O₄
Molecular Weight:714.98
Hs Code.:

C<sub>41</sub>H<sub>64</sub>F<sub>2</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:C₄₁H₆₄F₂N₄O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₆₄F₂N₄O₄

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Technology Process of C₄₁H₆₄F₂N₄O₄

There total 10 articles about C₄₁H₆₄F₂N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1271776-64-7
C₅₁H₈₂F₂N₄O₇

: 1271776-74-9
C₄₁H₆₄F₂N₄O₄

Guidance literature:: C₅₁H₈₂F₂N₄O₇; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 6h;

With sodium carbonate decahydrate; In dichloromethane; for 0.5h;

Reference yield:

: 32133-38-3,266360-61-6
2,5-difluoro-DL-phenylalanine

: 1271776-74-9
C₄₁H₆₄F₂N₄O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / Heating; Reflux

1.2: 0.5 h / 0 - 20 °C

2.1: triethylamine / dichloromethane / 20 °C

3.1: N,N-dimethyl-formamide / 18 h / 60 °C

4.1: sodium hydroxide; water / 6 h / 100 °C / Reflux

4.2: 20 °C

4.3: 18 h / 20 °C

5.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

5.2: 18 h / 0 - 20 °C

6.1: potassium iodide; sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

7.1: trifluoroacetic acid / dichloromethane / 6 h / 20 °C

7.2: 0.5 h

With lithium aluminium tetrahydride; water; sodium hydride; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; potassium iodide; sodium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 7328-91-8
2,2-Dimethyl-1,3-diaminopropane

: 1271776-74-9
C₄₁H₆₄F₂N₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

1.2: 18 h / 0 - 20 °C

2.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

2.2: 18 h / 0 - 20 °C

3.1: potassium iodide; sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 6 h / 20 °C

4.2: 0.5 h

With sodium hydride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; potassium iodide; In dichloromethane; N,N-dimethyl-formamide;