lauryl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,4-di-O-acetyl-3-O-allyl-β-D-glucopyranoside

Base Information

Chemical Name:lauryl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,4-di-O-acetyl-3-O-allyl-β-D-glucopyranoside
CAS No.:610316-61-5
Molecular Formula:C₅₉H₇₀O₁₇
Molecular Weight:1051.19
Hs Code.:

Synonyms:lauryl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,4-di-O-acetyl-3-O-allyl-β-D-glucopyranoside

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Chemical Property of lauryl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,4-di-O-acetyl-3-O-allyl-β-D-glucopyranoside

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Technology Process of lauryl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,4-di-O-acetyl-3-O-allyl-β-D-glucopyranoside

There total 11 articles about lauryl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,4-di-O-acetyl-3-O-allyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 112-53-8
1-dodecyl alcohol

: 524712-45-6
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,4-di-O-acetyl-3-O-allyl-α-D-glucopyranosyl trichloroacetimidate

: 610316-61-5
lauryl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,4-di-O-acetyl-3-O-allyl-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/S0968-0896(03)00118-4

Reference yield:

: 2592-58-7,3006-48-2,3006-49-3,13526-09-5,14679-57-3,22415-91-4,29884-70-6,41545-55-5,41545-56-6,41569-33-9,96996-90-6,121570-85-2,121570-86-3
1,2,3,4,6-penta-O-benzoyl-D-glucopyranoside

: 610316-61-5
lauryl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,4-di-O-acetyl-3-O-allyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 8 steps

1: ammonia / tetrahydrofuran; methanol / 12 h / 20 °C

2: 46 g / K₂CO₃ / CH₂Cl₂ / 24 h / 20 °C

3: 84 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 3 h / 20 °C

4: acetic acid / H₂O / 5 h / Heating

5: pyridine / 2 h / 20 °C

6: ammonia / tetrahydrofuran; methanol / 3 h / 20 °C

7: 11 g / K₂CO₃ / CH₂Cl₂ / 24 h / 20 °C

8: 92 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 3 h / 20 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; ammonia; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/S0968-0896(03)00118-4

Reference yield:

: 2280-44-6
D-Glucose

: 610316-61-5
lauryl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,4-di-O-acetyl-3-O-allyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 9 steps

1: NaH / dimethylformamide / 2 h / 20 °C

2: 7.1 g / acetic acid / H₂O / 24 h / 40 °C

3: 84 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 3 h / 20 °C

4: acetic acid / H₂O / 5 h / Heating

5: pyridine / 2 h / 20 °C

6: ammonia / tetrahydrofuran; methanol / 3 h / 20 °C

7: 11 g / K₂CO₃ / CH₂Cl₂ / 24 h / 20 °C

8: 92 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 3 h / 20 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; ammonia; sodium hydride; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(03)00118-4