2,2-dimesitylvinyl dimesitylacetate

Base Information

• Chemical Name: 2,2-dimesitylvinyl dimesitylacetate
• CAS No.: 96040-96-9
• Molecular Formula: C₄₀H₄₆O₂
• Molecular Weight: 558.804

Synonyms:2,2-dimesitylvinyl dimesitylacetate

Chemical Property of 2,2-dimesitylvinyl dimesitylacetate

Chemical Property:

Purity/Quality:

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Technology Process of 2,2-dimesitylvinyl dimesitylacetate

There total 3 articles about 2,2-dimesitylvinyl dimesitylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(mesityl)ketene (87871-33-8) → 2,2-bis(2,4,6-trimethylphenyl)acetic acid (5740-42-1) + 2,2-dimesitylvinyl dimesitylacetate (96040-96-9)

Guidance literature:

With t-butyl bromide; lithium; In diethyl ether; at -18 ℃; for 2h;

DOI:10.1021/ja00298a042

Reference yield:

N,N,N,N,N,N-hexamethylphosphoric triamide (680-31-9) + bis(mesityl)ketene (87871-33-8) → 2,2-dimesityl-vinyl alcohol (54288-04-9) + N-ethyl-N-methyldimesitylacetamide (134335-04-9) + 2,2-dimesityl-1-<(bisdimethylamino)phosphoryl>ethenol (134335-05-0) + 2,2-dimesitylvinyl dimesitylacetate (96040-96-9)

Guidance literature:

With methyllithium; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given; 1) ether, 0 deg C, 10 min, 2) ether, 0 deg C, 1 h;

DOI:10.1021/jo00013a031

Reference yield:

N,N,N,N,N,N-hexamethylphosphoric triamide (680-31-9) + bis(mesityl)ketene (87871-33-8) → 2,2-dimesityl-vinyl alcohol (54288-04-9) + N,N-dimethyldimesitylacetamide (134359-13-0) + N-ethyl-N-methyldimesitylacetamide (134335-04-9) + 2,2-dimesitylvinyl dimesitylacetate (96040-96-9)

Guidance literature:

With methyllithium; In diethyl ether; Mechanism; Product distribution; multistep reaction; asymmetric ketene;;

DOI:10.1021/jo00013a031

upstream raw materials:

N,N,N,N,N,N-hexamethylphosphoric triamide

bis(mesityl)ketene

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