4-(3-AMINO-PHENYL)-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER

Base Information

• Chemical Name: 4-(3-AMINO-PHENYL)-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER
• CAS No.: 387827-19-2
• Molecular Formula: C16H24 N2 O2
• Molecular Weight: 276.379
• Mol file: 387827-19-2.mol

Synonyms:4-(3-Aminophenyl)piperidine-1-carboxylicacid tert-butyl ester; tert-Butyl 4-[3-aminophenyl]-1-piperidinecarboxylate

Chemical Property of 4-(3-AMINO-PHENYL)-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.551
• Boiling Point: 413.217°C at 760 mmHg
• PKA: 4.60±0.10(Predicted)
• Flash Point: 203.706°C
• Density: 1.1g/cm³
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

97% ^*data from raw suppliers

1-Boc-4-(3-aminophenyl)piperidine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(3-AMINO-PHENYL)-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER

There total 9 articles about 4-(3-AMINO-PHENYL)-PIPERIDINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

tert-butyl 4-(3-nitrophenyl)piperidine-1-carboxylate (1510865-58-3) → tert-butyl 4-[3-(amino)phenyl]-1-piperidinecarboxylate (387827-19-2)

Guidance literature:

With methanol; palladium 10% on activated carbon; at 20 - 30 ℃; for 4h;

Reference yield: 92.0%

→ tert-butyl 4-[3-(amino)phenyl]-1-piperidinecarboxylate (387827-19-2)

Guidance literature:

Reference yield: 88.1%

tert-butyl 1,2,3,6-tetrahydro-4-(3-nitrophenyl)pyridine-1-carboxylate (138647-55-9) → tert-butyl 4-[3-(amino)phenyl]-1-piperidinecarboxylate (387827-19-2)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 16h; under 2068.65 Torr; Inert atmosphere;

upstream raw materials:

tert-butyl 1,2,3,6-tetrahydro-4-(3-nitrophenyl)pyridine-1-carboxylate

tert-butyl 4-[3-(amino)phenyl]-1,2,3,6-tetrahydro-1-pyridinecarboxylate

isopropylamine

N-tert-butyloxycarbonylpiperidin-4-one

Downstream raw materials:

4-(3-aminophenyl)piperidine

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