α-tert-Butoxy-ο-(ethoxycarbony)octa[carbonyl(p-methoxybenzylimino)pentamethylene]

Base Information

• Chemical Name: α-tert-Butoxy-ο-(ethoxycarbony)octa[carbonyl(p-methoxybenzylimino)pentamethylene]
• CAS No.: 200713-68-4
• Molecular Formula: C₁₁₉H₁₆₆N₈O₁₉
• Molecular Weight: 2012.67

Synonyms:α-tert-Butoxy-ο-(ethoxycarbony)octa[carbonyl(p-methoxybenzylimino)pentamethylene]

Chemical Property of α-tert-Butoxy-ο-(ethoxycarbony)octa[carbonyl(p-methoxybenzylimino)pentamethylene]

Chemical Property:

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Technology Process of α-tert-Butoxy-ο-(ethoxycarbony)octa[carbonyl(p-methoxybenzylimino)pentamethylene]

There total 1 articles about α-tert-Butoxy-ο-(ethoxycarbony)octa[carbonyl(p-methoxybenzylimino)pentamethylene] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

6-((4-Methoxy-benzyl)-{6-[(4-methoxy-benzyl)-(6-{(4-methoxy-benzyl)-[6-(4-methoxy-benzylamino)-hexanoyl]-amino}-hexanoyl)-amino]-hexanoyl}-amino)-hexanoic acid ethyl ester (200713-66-2) + 6-[{6-[{6-[{6-[tert-Butoxycarbonyl-(4-methoxy-benzyl)-amino]-hexanoyl}-(4-methoxy-benzyl)-amino]-hexanoyl}-(4-methoxy-benzyl)-amino]-hexanoyl}-(4-methoxy-benzyl)-amino]-hexanoic acid (200713-67-3) → α-tert-Butoxy-ο-(ethoxycarbony)octa[carbonyl(p-methoxybenzylimino)pentamethylene] (200713-68-4)

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature; 1.) 1.5 h, 2.) 48;

Reference yield: 91.0%

α-tert-Butoxy-ο-(ethoxycarbony)octa[carbonyl(p-methoxybenzylimino)pentamethylene] (200713-68-4) → ο-Ethoxyocta[(p-methoxybenzylimino)(6-oxohexamethylene)] (200713-69-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 5h; Ambient temperature;

Reference yield: 67.0%

α-tert-Butoxy-ο-(ethoxycarbony)octa[carbonyl(p-methoxybenzylimino)pentamethylene] (200713-68-4) → α-tert-Butoxy-ω-carboxyocta[carbonyl(p-methoxybenzylimino)pentamethylene]

Guidance literature:

With sodium hydroxide; In ethanol; at 120 ℃; for 0.166667h;

upstream raw materials:

6-((4-Methoxy-benzyl)-{6-[(4-methoxy-benzyl)-(6-{(4-methoxy-benzyl)-[6-(4-methoxy-benzylamino)-hexanoyl]-amino}-hexanoyl)-amino]-hexanoyl}-amino)-hexanoic acid ethyl ester

6-[{6-[{6-[{6-[tert-Butoxycarbonyl-(4-methoxy-benzyl)-amino]-hexanoyl}-(4-methoxy-benzyl)-amino]-hexanoyl}-(4-methoxy-benzyl)-amino]-hexanoyl}-(4-methoxy-benzyl)-amino]-hexanoic acid

Downstream raw materials:

ο-Ethoxyocta[(p-methoxybenzylimino)(6-oxohexamethylene)]

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