ethyl 5-(3,4-dichlorophenyl)-1-(phenylmethyl)-1,2,3,6-tetrahydro-4-pyridinecarboxylate

Base Information

Chemical Name:ethyl 5-(3,4-dichlorophenyl)-1-(phenylmethyl)-1,2,3,6-tetrahydro-4-pyridinecarboxylate
CAS No.:860473-03-6
Molecular Formula:C₂₁H₂₁Cl₂NO₂
Molecular Weight:390.309
Hs Code.:

Synonyms:ethyl 5-(3,4-dichlorophenyl)-1-(phenylmethyl)-1,2,3,6-tetrahydro-4-pyridinecarboxylate

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Chemical Property of ethyl 5-(3,4-dichlorophenyl)-1-(phenylmethyl)-1,2,3,6-tetrahydro-4-pyridinecarboxylate

Chemical Property:

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Technology Process of ethyl 5-(3,4-dichlorophenyl)-1-(phenylmethyl)-1,2,3,6-tetrahydro-4-pyridinecarboxylate

There total 3 articles about ethyl 5-(3,4-dichlorophenyl)-1-(phenylmethyl)-1,2,3,6-tetrahydro-4-pyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 151169-75-4
3,4-dichlophenylboronic acid

: 497843-21-7
1-benzyl-5-(trifluoromethanesulfonoyloxy)-3,6-dihydro-2H-pyridine-4-carboxylic acid ethyl ester

: 860473-03-6
ethyl 5-(3,4-dichlorophenyl)-1-(phenylmethyl)-1,2,3,6-tetrahydro-4-pyridinecarboxylate

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; toluene; at 100 ℃; for 14h;

Reference yield:

: 1010684-91-9
4-butanoyl-1-(phenylmethyl)-1,2,5,6-tetrahydro-3-pyridinyl-trifluoromethanesulfonate

: 151169-75-4
3,4-dichlophenylboronic acid

: 860473-03-6
ethyl 5-(3,4-dichlorophenyl)-1-(phenylmethyl)-1,2,3,6-tetrahydro-4-pyridinecarboxylate

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; at 80 ℃; for 5h;

Reference yield:

: 1010684-90-8
4-butanoyl-3-oxo-1-(phenylmethyl)piperidinium chloride

: 860473-03-6
ethyl 5-(3,4-dichlorophenyl)-1-(phenylmethyl)-1,2,3,6-tetrahydro-4-pyridinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 4 h / 20 °C

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 5 h / 80 °C

With sodium hydride; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; N,N-dimethyl-formamide;