4-butanoyl-1-(phenylmethyl)-1,2,5,6-tetrahydro-3-pyridinyl-trifluoromethanesulfonate

Base Information

Chemical Name:4-butanoyl-1-(phenylmethyl)-1,2,5,6-tetrahydro-3-pyridinyl-trifluoromethanesulfonate
CAS No.:1010684-91-9
Molecular Formula:C₁₇H₂₀F₃NO₄S
Molecular Weight:391.411
Hs Code.:

Synonyms:4-butanoyl-1-(phenylmethyl)-1,2,5,6-tetrahydro-3-pyridinyl-trifluoromethanesulfonate

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Chemical Property of 4-butanoyl-1-(phenylmethyl)-1,2,5,6-tetrahydro-3-pyridinyl-trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

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Technology Process of 4-butanoyl-1-(phenylmethyl)-1,2,5,6-tetrahydro-3-pyridinyl-trifluoromethanesulfonate

There total 1 articles about 4-butanoyl-1-(phenylmethyl)-1,2,5,6-tetrahydro-3-pyridinyl-trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 1010684-90-8
4-butanoyl-3-oxo-1-(phenylmethyl)piperidinium chloride

: 1010684-91-9
4-butanoyl-1-(phenylmethyl)-1,2,5,6-tetrahydro-3-pyridinyl-trifluoromethanesulfonate

Guidance literature:: 4-butanoyl-3-oxo-1-(phenylmethyl)piperidinium chloride; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

N,N-phenylbistrifluoromethane-sulfonimide; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

Reference yield:

: 1010684-91-9
4-butanoyl-1-(phenylmethyl)-1,2,5,6-tetrahydro-3-pyridinyl-trifluoromethanesulfonate

: 151169-75-4
3,4-dichlophenylboronic acid

: 860473-03-6
ethyl 5-(3,4-dichlorophenyl)-1-(phenylmethyl)-1,2,3,6-tetrahydro-4-pyridinecarboxylate

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; at 80 ℃; for 5h;

Reference yield:

: 1010684-91-9
4-butanoyl-1-(phenylmethyl)-1,2,5,6-tetrahydro-3-pyridinyl-trifluoromethanesulfonate

: 1010685-09-2
(1S,6S)-(3,4-dichlorophenyl)-6-[(methyloxy)methyl]-3-azabicyclo[4.1.0]heptane

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane / 5 h / 80 °C

2.1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 5 h / 50 °C

3.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran; toluene / 2 h / -20 °C

5.1: diethylzinc / hexane; dichloromethane / 18.75 h / -20 - 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

6.2: 0 - 20 °C

6.3: 18 h / 20 °C

7.1: hydrogenchloride; water / 1,4-dioxane / 18 h / 90 °C

8.1: hydrogenchloride / diethyl ether; dichloromethane

9.1: isopropylamine / ethanol

With hydrogenchloride; lithium aluminium tetrahydride; carbonochloridic acid 1-chloro-ethyl ester; water; diethylzinc; sodium hydride; potassium carbonate; isopropylamine; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; diethyl ether; ethanol; hexane; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;