(1-benzenesulfonyl-1H-indol-2-yl)-[3-(1-Benzenesulfonyl-1H-indol-2-yl)phenyl]methane

Base Information

Chemical Name:(1-benzenesulfonyl-1H-indol-2-yl)-[3-(1-Benzenesulfonyl-1H-indol-2-yl)phenyl]methane
CAS No.:1158373-47-7
Molecular Formula:C₃₅H₂₆N₂O₄S₂
Molecular Weight:602.734
Hs Code.:

Synonyms:(1-benzenesulfonyl-1H-indol-2-yl)-[3-(1-Benzenesulfonyl-1H-indol-2-yl)phenyl]methane

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Chemical Property of (1-benzenesulfonyl-1H-indol-2-yl)-[3-(1-Benzenesulfonyl-1H-indol-2-yl)phenyl]methane

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Technology Process of (1-benzenesulfonyl-1H-indol-2-yl)-[3-(1-Benzenesulfonyl-1H-indol-2-yl)phenyl]methane

There total 6 articles about (1-benzenesulfonyl-1H-indol-2-yl)-[3-(1-Benzenesulfonyl-1H-indol-2-yl)phenyl]methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1158373-44-4
(1-benzenesulfonyl-1H-indol-2-yl)-[3-(1-benzenesulfonyl-1H-indol-2-yl)phenyl]methanol

: 1158373-47-7
(1-benzenesulfonyl-1H-indol-2-yl)-[3-(1-Benzenesulfonyl-1H-indol-2-yl)phenyl]methane

Guidance literature:: (1-benzenesulfonyl-1H-indol-2-yl)-[3-(1-benzenesulfonyl-1H-indol-2-yl)phenyl]methanol; With triethylsilane; In dichloromethane; for 0.5h;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: (1-(phenylsulfonyl)-1H-indol-2-yl)boronic acid

: 1158373-47-7
(1-benzenesulfonyl-1H-indol-2-yl)-[3-(1-Benzenesulfonyl-1H-indol-2-yl)phenyl]methane

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane

2: lithium diisopropyl amide / tetrahydrofuran / -78 °C

3: triethylsilane; trifluoroacetic acid / dichloromethane / 20 °C

With triethylsilane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; trifluoroacetic acid; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; 1: Suzuki coupling;
DOI:10.1007/s00280-010-1319-8

Reference yield:

: 40899-71-6
1-benzenesulfonylindole

: 1158373-47-7
(1-benzenesulfonyl-1H-indol-2-yl)-[3-(1-Benzenesulfonyl-1H-indol-2-yl)phenyl]methane

Guidance literature:: Multi-step reaction with 4 steps

1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane

3: lithium diisopropyl amide / tetrahydrofuran / -78 °C

4: triethylsilane; trifluoroacetic acid / dichloromethane / 20 °C

With triethylsilane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; trifluoroacetic acid; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; 2: Suzuki coupling;
DOI:10.1007/s00280-010-1319-8