Technology Process of C20H22O6
There total 8 articles about C20H22O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver carbonate;
In
toluene;
at 80 ℃;
for 6h;
chemoselective reaction;
DOI:10.1016/j.tet.2012.06.105
- Guidance literature:
-
Multi-step reaction with 6 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 23 h / 0 - 20 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 4.5 h / 20 °C
3: sodium hydride / tetrahydrofuran; mineral oil / 17 h / 0 - 20 °C
4: hydrogenchloride / water / 3 h / 0 - 50 °C
5: hydrogenchloride; water / 1,4-dioxane / 5 h / 90 °C
6: silver carbonate / toluene / 6 h / 80 °C
With
hydrogenchloride; tetrabutyl ammonium fluoride; water; sodium hydride; N-ethyl-N,N-diisopropylamine; silver carbonate;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; mineral oil;
6: Fetizon oxidation;
DOI:10.1016/j.tet.2012.06.105
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4.5 h / 20 °C
2: sodium hydride / tetrahydrofuran; mineral oil / 17 h / 0 - 20 °C
3: hydrogenchloride / water / 3 h / 0 - 50 °C
4: hydrogenchloride; water / 1,4-dioxane / 5 h / 90 °C
5: silver carbonate / toluene / 6 h / 80 °C
With
hydrogenchloride; tetrabutyl ammonium fluoride; water; sodium hydride; silver carbonate;
In
tetrahydrofuran; 1,4-dioxane; water; toluene; mineral oil;
5: Fetizon oxidation;
DOI:10.1016/j.tet.2012.06.105
