Technology Process of C24H29NO4S
There total 5 articles about C24H29NO4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
BF4(1-)*C16H22NO3S(1+);
With
sodium hydroxide;
In
water; tert-butyl alcohol;
at 25 ℃;
for 3h;
Inert atmosphere;
2-methylphenyl aldehyde;
In
water; tert-butyl alcohol;
optical yield given as %de;
Inert atmosphere;
DOI:10.1021/jo1025964
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / 0 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Inert atmosphere
3.1: acetonitrile / 12 h / 20 °C / Inert atmosphere
4.1: sodium hydroxide / water; tert-butyl alcohol / 3 h / 25 °C / Inert atmosphere
4.2: Inert atmosphere
With
n-butyllithium; boron trifluoride diethyl etherate; sodium hydroxide;
In
tetrahydrofuran; hexane; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1021/jo1025964
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Inert atmosphere
2.1: acetonitrile / 12 h / 20 °C / Inert atmosphere
3.1: sodium hydroxide / water; tert-butyl alcohol / 3 h / 25 °C / Inert atmosphere
3.2: Inert atmosphere
With
boron trifluoride diethyl etherate; sodium hydroxide;
In
dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1021/jo1025964
