5-Pyrimidinecarboxaldehyde, 4-amino-1,2-dihydro-1-methyl-2-oxo- (9CI)

Base Information

• Chemical Name: 5-Pyrimidinecarboxaldehyde, 4-amino-1,2-dihydro-1-methyl-2-oxo- (9CI)
• CAS No.: 387334-40-9
• Molecular Formula: C₆H₇N₃O₂
• Molecular Weight: 153.14
• Mol file: 387334-40-9.mol

Synonyms:5-Pyrimidinecarboxaldehyde, 4-amino-1,2-dihydro-1-methyl-2-oxo- (9CI)

Chemical Property of 5-Pyrimidinecarboxaldehyde, 4-amino-1,2-dihydro-1-methyl-2-oxo- (9CI)

Chemical Property:

• PSA: 77.98000
• LogP: -0.24380

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Pyrimidinecarboxaldehyde, 4-amino-1,2-dihydro-1-methyl-2-oxo- (9CI)

There total 4 articles about 5-Pyrimidinecarboxaldehyde, 4-amino-1,2-dihydro-1-methyl-2-oxo- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

1-methyl-5-hydroxymethylcytosine (1146966-36-0) → 1-methyl-5-formylcytosine (387334-40-9)

Guidance literature:

With manganese(IV) oxide; In acetonitrile; at 20 ℃; for 20h;

DOI:10.1002/cbic.202100651

Reference yield:

1,5-dimethylcytosine (17634-60-5) → 1-methyl-5-hydroxymethylcytosine (1146966-36-0) + 1-methyl-5-formylcytosine (387334-40-9) + C12H15N5O2

Guidance literature:

With water; at -78.5 ℃; UV-irradiation;

DOI:10.1111/j.1751-1097.2011.01070.x

Reference yield:

C6H9N3O3 → 1-methyl-5-formylcytosine (387334-40-9)

Guidance literature:

In water; at 22 ℃; pH=7.7; Equilibrium constant; Thermodynamic data;

DOI:10.1002/cbic.202100651

upstream raw materials:

1,5-dimethylcytosine

1-methyl-5-hydroxymethylcytosine

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