(1S,2R,3R,4R)-4-[(4-bromophenyl)carbonyloxy]-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-bromobenzoate

Base Information

Chemical Name:(1S,2R,3R,4R)-4-[(4-bromophenyl)carbonyloxy]-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-bromobenzoate
CAS No.:1559057-69-0
Molecular Formula:C₃₉H₄₀Br₂F₂O₇
Molecular Weight:818.547
Hs Code.:

(1S,2R,3R,4R)-4-[(4-bromophenyl)carbonyloxy]-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-bromobenzoate

Synonyms:(1S,2R,3R,4R)-4-[(4-bromophenyl)carbonyloxy]-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-bromobenzoate

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Chemical Property of (1S,2R,3R,4R)-4-[(4-bromophenyl)carbonyloxy]-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-bromobenzoate

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Technology Process of (1S,2R,3R,4R)-4-[(4-bromophenyl)carbonyloxy]-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-bromobenzoate

There total 4 articles about (1S,2R,3R,4R)-4-[(4-bromophenyl)carbonyloxy]-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-bromobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1559057-55-4
(1S,2R,3R,4R)-4-[(4-bromophenyl)carbonyloxy]-3-[(1E)-3-oxo-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-bromobenzoate

: 1559057-69-0
(1S,2R,3R,4R)-4-[(4-bromophenyl)carbonyloxy]-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-bromobenzoate

Guidance literature:: With pyridine hydrogenfluoride; In toluene; at 25 ℃; for 5h;

Reference yield:

: 1559057-77-0,130209-78-8
C₂₅H₃₆O₆

: 1559057-69-0
(1S,2R,3R,4R)-4-[(4-bromophenyl)carbonyloxy]-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-bromobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; 1,4-dioxane / 11 h / 25 - 40 °C

2: pyridine / dichloromethane / 4 h / 5 - 25 °C

3: pyridine hydrogenfluoride / toluene / 5 h / 25 °C

With pyridine; pyridine hydrogenfluoride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; dichloromethane; toluene;

Reference yield:

: 1559057-74-7
(Z)-isopropyl 7-((1R,5S,6R,7R)-7-((E)-3-hydroxy-4-phenoxybut-1-en-1-yl)-3-phenyl-2,4-dioxa-3-borabicyclo[3.2.1]octan-6-yl)hept-5-enoate

: 1559057-69-0
(1S,2R,3R,4R)-4-[(4-bromophenyl)carbonyloxy]-3-[(1E)-3,3-difluoro-4-phenoxybut-1-en-1-yl]-2-[(2Z)-7-oxo-7-(propan-2-yloxy)hept-2-en-1-yl]cyclopentyl 4-bromobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: PCC on alumina / dichloromethane / 3 h / 25 °C

2: pyridine / dichloromethane / 4 h / 5 - 25 °C

3: pyridine hydrogenfluoride / toluene / 5 h / 25 °C

With pyridine; PCC on alumina; pyridine hydrogenfluoride; In dichloromethane; toluene;