Rh₂(C₆H₄(PCH₃C₆H₅)2)2⁽²⁺⁾*2PF₆^(1-)*CH₂Cl₂=Rh₂(C₆H₄(PCH₃C₆H₅)2)2(PF₆)2*CH₂Cl₂

Base Information

• Chemical Name: Rh₂(C₆H₄(PCH₃C₆H₅)2)2⁽²⁺⁾*2PF₆^(1-)*CH₂Cl₂=Rh₂(C₆H₄(PCH₃C₆H₅)2)2(PF₆)2*CH₂Cl₂
• CAS No.: 100946-01-8
• Molecular Formula: CH₂Cl₂*C₄₀H₄₀P₄Rh₂*2F₆P
• Molecular Weight: 1225.32
• Mol file: 100946-01-8.mol

Synonyms:Rh₂(C₆H₄(PCH₃C₆H₅)2)2⁽²⁺⁾*2PF₆^(1-)*CH₂Cl₂=Rh₂(C₆H₄(PCH₃C₆H₅)2)2(PF₆)2*CH₂Cl₂

Chemical Property of Rh₂(C₆H₄(PCH₃C₆H₅)2)2⁽²⁺⁾*2PF₆^(1-)*CH₂Cl₂=Rh₂(C₆H₄(PCH₃C₆H₅)2)2(PF₆)2*CH₂Cl₂

Chemical Property:

Purity/Quality:

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Technology Process of Rh₂(C₆H₄(PCH₃C₆H₅)2)2⁽²⁺⁾*2PF₆^(1-)*CH₂Cl₂=Rh₂(C₆H₄(PCH₃C₆H₅)2)2(PF₆)2*CH₂Cl₂

There total 1 articles about Rh₂(C₆H₄(PCH₃C₆H₅)2)2⁽²⁺⁾*2PF₆^(1-)*CH₂Cl₂=Rh₂(C₆H₄(PCH₃C₆H₅)2)2(PF₆)2*CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

[R-(R*,R*)]-(bicyclo[2.2.1]hepta-2,5-diene)[1,2-phenylenebis(methylphenylphosphine)]rhodium(I) hexafluorophosphate*diacetone (100945-97-9) → Rh2(C6H4(PCH3C6H5)2)2(2+)*2PF6(1-)*CH2Cl2=Rh2(C6H4(PCH3C6H5)2)2(PF6)2*CH2Cl2 (100946-01-8)

Guidance literature:

With hydrogen; In dichloromethane; a soln. of Rh complex was stirred under 1 atm H2 for 15 h; filtn., recrystn. from hot CH2Cl2, elem. anal.;

DOI:10.1021/om00136a029

upstream raw materials:

[R-(R*,R*)]-(bicyclo[2.2.1]hepta-2,5-diene)[1,2-phenylenebis(methylphenylphosphine)]rhodium(I) hexafluorophosphate*diacetone