4-(5'-hydroxy-2'-methoxycarbonyl-3'-methylphenoxy)-2-methoxy-6-methylbenzoic acid

Base Information

Chemical Name:4-(5'-hydroxy-2'-methoxycarbonyl-3'-methylphenoxy)-2-methoxy-6-methylbenzoic acid
CAS No.:132281-68-6
Molecular Formula:C₁₈H₁₈O₇
Molecular Weight:346.337
Hs Code.:

Synonyms:4-(5'-hydroxy-2'-methoxycarbonyl-3'-methylphenoxy)-2-methoxy-6-methylbenzoic acid

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Chemical Property of 4-(5'-hydroxy-2'-methoxycarbonyl-3'-methylphenoxy)-2-methoxy-6-methylbenzoic acid

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Technology Process of 4-(5'-hydroxy-2'-methoxycarbonyl-3'-methylphenoxy)-2-methoxy-6-methylbenzoic acid

There total 1 articles about 4-(5'-hydroxy-2'-methoxycarbonyl-3'-methylphenoxy)-2-methoxy-6-methylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 132281-67-5
methyl 4-benzyloxy-2-(4'-benzyloxycarbonyl-3'-methoxy-5'-methylphenoxy)-6-methylbenzoate

: 132281-68-6
4-(5'-hydroxy-2'-methoxycarbonyl-3'-methylphenoxy)-2-methoxy-6-methylbenzoic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 16h;
DOI:10.1071/CH9902107

Reference yield: 98.0%

: 100-39-0
benzyl bromide

: 132281-68-6
4-(5'-hydroxy-2'-methoxycarbonyl-3'-methylphenoxy)-2-methoxy-6-methylbenzoic acid

: 132281-69-7
methyl 2-(4'-benzyloxycarbonyl-3'-methoxy-5'-methylphenoxy)-4-hydroxy-6-methylbenzoate

Guidance literature:: With potassium hydrogencarbonate; In N,N-dimethyl-formamide; for 16h; Ambient temperature;
DOI:10.1071/CH9902107

Reference yield:

: 132281-68-6
4-(5'-hydroxy-2'-methoxycarbonyl-3'-methylphenoxy)-2-methoxy-6-methylbenzoic acid

: 132281-71-1
benzyl 9-hydroxy-3-methoxy-6-methoxycarbonyl-1,7-dimethyldibenzofuran-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / KHCO₃ / dimethylformamide / 16 h / Ambient temperature

2: 19 percent / Pd(OAc)2, CF₃COOH / acetic acid / 16 h / Ambient temperature

With palladium diacetate; potassium hydrogencarbonate; trifluoroacetic acid; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1071/CH9902107