1,1,1,4,4,4-hexaphenyltetramethyltetrasilane

Base Information

Chemical Name:1,1,1,4,4,4-hexaphenyltetramethyltetrasilane
CAS No.:25368-92-7
Molecular Formula:C₄₀H₄₂Si₄
Molecular Weight:635.115
Hs Code.:

Synonyms:1,1,1,4,4,4-hexaphenyltetramethyltetrasilane

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Chemical Property of 1,1,1,4,4,4-hexaphenyltetramethyltetrasilane

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Technology Process of 1,1,1,4,4,4-hexaphenyltetramethyltetrasilane

There total 2 articles about 1,1,1,4,4,4-hexaphenyltetramethyltetrasilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 4342-61-4
1,2-dichlorotetramethylsilane

: 76-86-8
Triphenylsilyl chloride

: 25368-92-7
1,1,1,4,4,4-hexaphenyltetramethyltetrasilane

Guidance literature:: With lithium; In toluene; at -30 - 20 ℃; for 0.5h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.organomet.9b00507

Reference yield:

: 25368-92-7
1,1,1,4,4,4-hexaphenyltetramethyltetrasilane

Guidance literature:: Triphenylsilyl-lithium, Dichlortetramethyldisilan;
DOI:10.1016/S0022-328X(00)88610-6

Reference yield: 95.0%

: 1493-13-6
trifluorormethanesulfonic acid

: 25368-92-7
1,1,1,4,4,4-hexaphenyltetramethyltetrasilane

: 1,1',4,4'-tetraphenyltetramethyltetrasilane-1,4-bis(trifluoromethane-sulfonate)

Guidance literature:: With lithium; In toluene; at -80 - 20 ℃; for 2.16667h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.organomet.9b00507