2-Phenylpyrimidine-4,6-dicarboxaldehyde, bis[methyl[6-[1-methyl-2-(6-hydroxy-methylacryloylpyridin-2-ylmethyl-ene)-hydrazino]-2-methylpyrimidin-4-yl]hydrazone]

Base Information

Chemical Name:2-Phenylpyrimidine-4,6-dicarboxaldehyde, bis[methyl[6-[1-methyl-2-(6-hydroxy-methylacryloylpyridin-2-ylmethyl-ene)-hydrazino]-2-methylpyrimidin-4-yl]hydrazone]
CAS No.:1610456-62-6
Molecular Formula:C₄₆H₄₆N₁₆O₄
Molecular Weight:886.976
Hs Code.:

2-Phenylpyrimidine-4,6-dicarboxaldehyde, bis[methyl[6-[1-methyl-2-(6-hydroxy-methylacryloylpyridin-2-ylmethyl-ene)-hydrazino]-2-methylpyrimidin-4-yl]hydrazone]

Synonyms:2-Phenylpyrimidine-4,6-dicarboxaldehyde, bis[methyl[6-[1-methyl-2-(6-hydroxy-methylacryloylpyridin-2-ylmethyl-ene)-hydrazino]-2-methylpyrimidin-4-yl]hydrazone]

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Chemical Property of 2-Phenylpyrimidine-4,6-dicarboxaldehyde, bis[methyl[6-[1-methyl-2-(6-hydroxy-methylacryloylpyridin-2-ylmethyl-ene)-hydrazino]-2-methylpyrimidin-4-yl]hydrazone]

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Technology Process of 2-Phenylpyrimidine-4,6-dicarboxaldehyde, bis[methyl[6-[1-methyl-2-(6-hydroxy-methylacryloylpyridin-2-ylmethyl-ene)-hydrazino]-2-methylpyrimidin-4-yl]hydrazone]

There total 6 articles about 2-Phenylpyrimidine-4,6-dicarboxaldehyde, bis[methyl[6-[1-methyl-2-(6-hydroxy-methylacryloylpyridin-2-ylmethyl-ene)-hydrazino]-2-methylpyrimidin-4-yl]hydrazone] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1610456-61-5
2-Phenylpyrimidine-4,6-dicarboxaldehyde, bis[methyl[6-[1-methyl-2-(6-hydroxy-methylpyridin-2-ylmethylene)-hydrazino]-2-methylpyrimidin-4-yl]hydrazone]

: 814-68-6,25189-84-8
acryloyl chloride

: 1610456-62-6
2-Phenylpyrimidine-4,6-dicarboxaldehyde, bis[methyl[6-[1-methyl-2-(6-hydroxy-methylacryloylpyridin-2-ylmethyl-ene)-hydrazino]-2-methylpyrimidin-4-yl]hydrazone]

Guidance literature:: With triethylamine; In dichloromethane; at 60 ℃; for 4h; Inert atmosphere;
DOI:10.1039/c3dt53559b

Reference yield:

: 14164-34-2
4,6-dimethyl-2-phenylpyrimidine

: 1610456-62-6
2-Phenylpyrimidine-4,6-dicarboxaldehyde, bis[methyl[6-[1-methyl-2-(6-hydroxy-methylacryloylpyridin-2-ylmethyl-ene)-hydrazino]-2-methylpyrimidin-4-yl]hydrazone]

Guidance literature:: Multi-step reaction with 3 steps

1: iodine; trifluoroacetic acid / dimethyl sulfoxide / 2 h / 150 °C

2: ethanol / 6 h / Reflux

3: triethylamine / dichloromethane / 4 h / 60 °C / Inert atmosphere

With iodine; triethylamine; trifluoroacetic acid; In ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1039/c3dt53559b

Reference yield:

: 80109-86-0
2-phenyl-4,6-pyrimidinedicarboxaldehyde

: 1610456-62-6
2-Phenylpyrimidine-4,6-dicarboxaldehyde, bis[methyl[6-[1-methyl-2-(6-hydroxy-methylacryloylpyridin-2-ylmethyl-ene)-hydrazino]-2-methylpyrimidin-4-yl]hydrazone]

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 6 h / Reflux

2: triethylamine / dichloromethane / 4 h / 60 °C / Inert atmosphere

With triethylamine; In ethanol; dichloromethane;
DOI:10.1039/c3dt53559b