(R)-N-(tert-butylsulfonyl)-α-(trimethylstannyl)benzylamine

Base Information

Chemical Name:(R)-N-(tert-butylsulfonyl)-α-(trimethylstannyl)benzylamine
CAS No.:1610353-86-0
Molecular Formula:C₁₄H₂₅NO₂SSn
Molecular Weight:390.134
Hs Code.:

Synonyms:(R)-N-(tert-butylsulfonyl)-α-(trimethylstannyl)benzylamine

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Chemical Property of (R)-N-(tert-butylsulfonyl)-α-(trimethylstannyl)benzylamine

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Technology Process of (R)-N-(tert-butylsulfonyl)-α-(trimethylstannyl)benzylamine

There total 2 articles about (R)-N-(tert-butylsulfonyl)-α-(trimethylstannyl)benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1621881-50-2
C₁₄H₂₅NOSSn

: 1610353-86-0
(R)-N-(tert-butylsulfonyl)-α-(trimethylstannyl)benzylamine

Guidance literature:: With peracetic acid; In dichloromethane; at 20 ℃; for 0.333333h;
DOI:10.1021/ol501143c

Reference yield:

: 196929-85-8
(R)-N-benzylidene-2-methylpropane-2-sulfinamide

: 1610353-86-0
(R)-N-(tert-butylsulfonyl)-α-(trimethylstannyl)benzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium; diethylzinc / tetrahydrofuran / 0.5 h / -78 °C

2: peracetic acid / dichloromethane / 0.33 h / 20 °C

With peracetic acid; n-butyllithium; diethylzinc; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol501143c

Reference yield: 53.0%

: 124-38-9,18923-20-1
carbon dioxide

: 1610353-86-0
(R)-N-(tert-butylsulfonyl)-α-(trimethylstannyl)benzylamine

: 1610353-91-7
C₁₂H₁₇NO₄S

: 1563551-09-6
C₁₂H₁₇NO₄S

Guidance literature:: carbon dioxide; With cesium fluoride; In Triethylene glycol dimethyl ether; under 7600.51 Torr;

(R)-N-(tert-butylsulfonyl)-α-(trimethylstannyl)benzylamine; In Triethylene glycol dimethyl ether; at 100 ℃; for 3h;

With hydrogenchloride; In Triethylene glycol dimethyl ether; water; pH=2;
DOI:10.1021/ol501143c