Technology Process of C17H27NO2S
There total 8 articles about C17H27NO2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: trifluoroacetic acid / dichloromethane / 15 h / Reflux
2: triethylamine / dichloromethane / 2 h / 0 °C
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C
4: hydrogen; hydrogenchloride; palladium on activated charcoal / methanol; water / 15 h / 2585.81 Torr / Inert atmosphere
5: hydrogenchloride / water / 24 h / Reflux
6: potassium carbonate / acetonitrile / 15 h / Reflux
With
hydrogenchloride; palladium on activated charcoal; hydrogen; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;
In
methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.ejmech.2012.12.031
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C
2: hydrogen; hydrogenchloride; palladium on activated charcoal / methanol; water / 15 h / 2585.81 Torr / Inert atmosphere
3: hydrogenchloride / water / 24 h / Reflux
4: potassium carbonate / acetonitrile / 15 h / Reflux
With
hydrogenchloride; palladium on activated charcoal; hydrogen; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.ejmech.2012.12.031
