C₂₃H₃₁N₂O₈PS

Base Information

• Chemical Name: C₂₃H₃₁N₂O₈PS
• CAS No.: 126451-36-3
• Molecular Formula: C₂₃H₃₁N₂O₈PS
• Molecular Weight: 526.548
• Mol file: 126451-36-3.mol

Synonyms:C₂₃H₃₁N₂O₈PS

Chemical Property of C₂₃H₃₁N₂O₈PS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₃₁N₂O₈PS

There total 4 articles about C₂₃H₃₁N₂O₈PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

methyl phenylphosphinate (7162-15-4,111469-75-1,121467-78-5) + methyl 2,3-O-isopropylidene-β-D-erythro-pentopyranosid-4-ulose (E,Z)-4-<(p-tolylsulfono)hydrazide> (87924-31-0,89361-63-7,89361-64-8,99436-67-6,99436-68-7,99436-69-8,99436-70-1) → C20H27N2O8PS + C23H31N2O8PS + C23H31N2O8PS (126451-36-3) + C23H31N2O8PS

Guidance literature:

With trifluorormethanesulfonic acid; at 25 ℃; for 5h;

DOI:10.1246/bcsj.62.2320

Reference yield:

2,2-dimethoxy-propane (77-76-9) + C20H27N2O8PS → C23H31N2O8PS + C23H31N2O8PS (126451-36-3) + C23H31N2O8PS

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 25 ℃; for 8h; Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1246/bcsj.62.2320

Reference yield:

methyl phenylphosphinate (7162-15-4,111469-75-1,121467-78-5) → C23H31N2O8PS (126451-36-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 9 percent / triflic acid / 10 h / 20 °C

2: 4M HCl / dioxane / 8 h / 25 °C

With hydrogenchloride; trifluorormethanesulfonic acid; In 1,4-dioxane;

DOI:10.1246/bcsj.62.2320

upstream raw materials:

methyl phenylphosphinate

methyl 2,3-O-isopropylidene-β-D-erythro-pentopyranosid-4-ulose (E,Z)-4-<(p-tolylsulfono)hydrazide>

2,2-dimethoxy-propane