3,5-di-O-benzyl-4-C-(2-t-butyldiphenylsilyloxyethyl)1,2-di-O-acetyl-α-D-erythropentofuranose

Base Information

Chemical Name:3,5-di-O-benzyl-4-C-(2-t-butyldiphenylsilyloxyethyl)1,2-di-O-acetyl-α-D-erythropentofuranose
CAS No.:1300590-32-2
Molecular Formula:C₄₁H₄₈O₈Si
Molecular Weight:696.913
Hs Code.:

Synonyms:3,5-di-O-benzyl-4-C-(2-t-butyldiphenylsilyloxyethyl)1,2-di-O-acetyl-α-D-erythropentofuranose

Suppliers and Price of 3,5-di-O-benzyl-4-C-(2-t-butyldiphenylsilyloxyethyl)1,2-di-O-acetyl-α-D-erythropentofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-di-O-benzyl-4-C-(2-t-butyldiphenylsilyloxyethyl)1,2-di-O-acetyl-α-D-erythropentofuranose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3,5-di-O-benzyl-4-C-(2-t-butyldiphenylsilyloxyethyl)1,2-di-O-acetyl-α-D-erythropentofuranose

There total 6 articles about 3,5-di-O-benzyl-4-C-(2-t-butyldiphenylsilyloxyethyl)1,2-di-O-acetyl-α-D-erythropentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1300590-29-7
3,5-di-O-benzyl-4-(2-t-butyldiphenylsilyloxyethyl)-1,2-O-isopropylidene-α-D-erythropentofuranose

: 108-24-7
acetic anhydride

: 1300590-32-2
3,5-di-O-benzyl-4-C-(2-t-butyldiphenylsilyloxyethyl)1,2-di-O-acetyl-α-D-erythropentofuranose

Guidance literature:: With sulfuric acid; In acetic acid; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.bmc.2013.04.049

Reference yield: 91.0%

: 1300590-29-7
3,5-di-O-benzyl-4-(2-t-butyldiphenylsilyloxyethyl)-1,2-O-isopropylidene-α-D-erythropentofuranose

: 1300590-32-2
3,5-di-O-benzyl-4-C-(2-t-butyldiphenylsilyloxyethyl)1,2-di-O-acetyl-α-D-erythropentofuranose

Guidance literature:: With sulfuric acid; acetic anhydride; acetic acid; at 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 287737-62-6
2-((3aR,5R,6S,6aR)-6-(benzyloxy)-5-((benzyloxy)methyl)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)ethanol

: 1300590-32-2
3,5-di-O-benzyl-4-C-(2-t-butyldiphenylsilyloxyethyl)1,2-di-O-acetyl-α-D-erythropentofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

2: acetic anhydride; sulfuric acid; acetic acid / 2 h / 20 °C / Inert atmosphere

With dmap; sulfuric acid; acetic anhydride; acetic acid; triethylamine; In dichloromethane;