(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)IrCl

Base Information

Chemical Name:(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)IrCl
CAS No.:1332882-70-8
Molecular Formula:C₂₁H₁₅Cl₅IrN₃
Molecular Weight:678.855
Hs Code.:

(NC<sub>5</sub>H<sub>3</sub>(C(CH<sub>3</sub>)NC<sub>6</sub>H<sub>3</sub>Cl<sub>2</sub>)2)IrCl

Synonyms:(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)IrCl

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Chemical Property of (NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)IrCl

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Technology Process of (NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)IrCl

There total 1 articles about (NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)IrCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 323179-70-0
2,6-bis[1-(2,6-dichlorophenylimino)ethyl]pyridine

: 39722-81-1
di-μ-chlorotetrakis(ethene)diiridium(I)

: 1332882-70-8
(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)IrCl

Guidance literature:: In tetrahydrofuran; diethyl ether; (N2) to soln. ligand in THF soln. Ir complex in Et2O was added, stirred for 1 h; solvent was removed in vacuo, residue was washed with THF-Et2O (1:1) andpentane and dried in vacuo for several hours; elem. anal.;
DOI:10.1039/c1dt10886g

Reference yield: 86.0%

: 1332882-70-8
(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)IrCl

: 124-41-4
sodium methylate

: 1332882-71-9
(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)Ir(OCH₃)

Guidance literature:: In tetrahydrofuran; methanol; (N2) suspn. Ir complex and MeONa in MeOH-THF was stirred for 16 h; solvents were removed in vacuo, residual solvents were co-evaporated with pentane, dried in vacuo and extd. into toluene, soln. was evapd.; elem. anal.;
DOI:10.1039/c1dt10886g

Reference yield:

: 1332882-70-8
(NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)IrCl

: (NC₅H₃(C(CH₃)NC₆H₃Cl₂)2)IrN

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; methanol

2: tetrahydrofuran

3: neat (no solvent, solid phase)

In tetrahydrofuran; methanol;
DOI:10.1039/c1dt10886g