2-hydroxy-3,9-dibenzyloxy-10-methoxy-13-n-octylprotoberberine chloride

Base Information

Chemical Name:2-hydroxy-3,9-dibenzyloxy-10-methoxy-13-n-octylprotoberberine chloride
CAS No.:1375475-85-6
Molecular Formula:C₄₀H₄₄NO₄*Cl
Molecular Weight:638.247
Hs Code.:

Synonyms:2-hydroxy-3,9-dibenzyloxy-10-methoxy-13-n-octylprotoberberine chloride

Suppliers and Price of 2-hydroxy-3,9-dibenzyloxy-10-methoxy-13-n-octylprotoberberine chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-hydroxy-3,9-dibenzyloxy-10-methoxy-13-n-octylprotoberberine chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-hydroxy-3,9-dibenzyloxy-10-methoxy-13-n-octylprotoberberine chloride

There total 4 articles about 2-hydroxy-3,9-dibenzyloxy-10-methoxy-13-n-octylprotoberberine chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 1375475-65-2
2,3,9-trihydroxyl-10-methoxy-13-n-octylprotoberberine chloride

: 100-39-0
benzyl bromide

: 1375475-85-6
2-hydroxy-3,9-dibenzyloxy-10-methoxy-13-n-octylprotoberberine chloride

Guidance literature:: 2,3,9-trihydroxyl-10-methoxy-13-n-octylprotoberberine chloride; benzyl bromide; With potassium hydroxide; In N,N-dimethyl-formamide; at 70 ℃;

With hydrogenchloride; In water;
DOI:10.1016/j.ejmech.2012.03.012

Reference yield:

: 483-15-8
7,8-dihydroberberine

: 1375475-85-6
2-hydroxy-3,9-dibenzyloxy-10-methoxy-13-n-octylprotoberberine chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / ethanol / 5 h / 85 - 95 °C

1.2: 0.5 h / 20 °C

2.1: aluminum (III) chloride / dichloromethane / 72 h / 20 °C

3.1: potassium hydroxide / N,N-dimethyl-formamide / 70 °C

With aluminum (III) chloride; acetic acid; potassium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.03.012

Reference yield:

: 633-65-8
berberine chloride

: 1375475-85-6
2-hydroxy-3,9-dibenzyloxy-10-methoxy-13-n-octylprotoberberine chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate; potassium carbonate; sodium hydroxide / methanol / 2 h / 20 °C

2.1: acetic acid / ethanol / 5 h / 85 - 95 °C

2.2: 0.5 h / 20 °C

3.1: aluminum (III) chloride / dichloromethane / 72 h / 20 °C

4.1: potassium hydroxide / N,N-dimethyl-formamide / 70 °C

With aluminum (III) chloride; sodium tetrahydroborate; potassium carbonate; acetic acid; potassium hydroxide; sodium hydroxide; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.03.012