C₉H₁₂BN

Base Information

• Chemical Name: C₉H₁₂BN
• CAS No.: 1610970-58-5
• Molecular Formula: C₉H₁₂BN
• Molecular Weight: 145.012
• Mol file: 1610970-58-5.mol

Synonyms:C₉H₁₂BN

Chemical Property of C₉H₁₂BN

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₉H₁₂BN

There total 4 articles about C₉H₁₂BN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

C10H11BN2 (1610970-47-2) → C9H12BN (1610970-58-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.75h;

DOI:10.1002/anie.201402614

Reference yield:

3-phenylprop-2-yn-1-amine hydrochloride (30011-36-0) → C9H12BN (1610970-58-5)

Guidance literature:

Multi-step reaction with 3 steps

1: magnesium sulfate / tetrahydrofuran / 24 h / Reflux

2: XPhosAu(triazole)OTf / 1,2-dichloro-ethane / 72 h / 80 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 0.75 h / 0 - 20 °C

With lithium aluminium tetrahydride; XPhosAu(triazole)OTf; magnesium sulfate; In tetrahydrofuran; 1,2-dichloro-ethane;

DOI:10.1002/anie.201402614

Reference yield:

2-(3-phenylprop-2-yn-1-yl)isoindoline-1,3-dione (4656-94-4) → C9H12BN (1610970-58-5)

Guidance literature:

Multi-step reaction with 4 steps

1.1: hydrazine hydrate / 45 °C

1.2: 0.25 h / 20 °C

2.1: magnesium sulfate / tetrahydrofuran / 24 h / Reflux

3.1: XPhosAu(triazole)OTf / 1,2-dichloro-ethane / 72 h / 80 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.75 h / 0 - 20 °C

With lithium aluminium tetrahydride; XPhosAu(triazole)OTf; magnesium sulfate; hydrazine hydrate; In tetrahydrofuran; 1,2-dichloro-ethane;

DOI:10.1002/anie.201402614

upstream raw materials:

C₁₀H₁₁BN₂

3-phenylprop-2-yn-1-amine hydrochloride

C₁₀H₁₁BN₂

2-(3-phenylprop-2-yn-1-yl)isoindoline-1,3-dione