3-(1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridin-3-yl)acrylic acid benzyl ester

Base Information

Chemical Name:3-(1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridin-3-yl)acrylic acid benzyl ester
CAS No.:1381963-87-6
Molecular Formula:C₂₂H₂₁NO₃
Molecular Weight:347.414
Hs Code.:

Synonyms:3-(1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridin-3-yl)acrylic acid benzyl ester

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Chemical Property of 3-(1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridin-3-yl)acrylic acid benzyl ester

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Technology Process of 3-(1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridin-3-yl)acrylic acid benzyl ester

There total 2 articles about 3-(1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridin-3-yl)acrylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 2495-35-4,25036-21-9
benzylacrylate

: 108046-33-9
1-benzyl-1,2,3,4-tetrahydro-2-pyridinone

: 1381963-87-6
3-(1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridin-3-yl)acrylic acid benzyl ester

Guidance literature:: With oxygen; palladium diacetate; copper(II) acetate monohydrate; acetic acid; In N,N-dimethyl acetamide; at 70 ℃; for 3h; stereoselective reaction;
DOI:10.1021/ol301249n

Reference yield:

: C₂₂H₂₁NO₄

: 1381963-87-6
3-(1-benzyl-6-oxo-1,4,5,6-tetrahydro-pyridin-3-yl)acrylic acid benzyl ester

Guidance literature:: C₂₂H₂₁NO₄; With lithium triethylborohydride; In tetrahydrofuran; toluene; at -78 ℃; for 1h; Inert atmosphere;

With dmap; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; In tetrahydrofuran; toluene; at -78 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1039/d0nj01209b