Technology Process of C57H100O9
There total 17 articles about C57H100O9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C50H94O9;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 ℃;
for 1h;
Inert atmosphere;
benzyl bromide;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1055/s-0032-1317929
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C / Inert atmosphere
2.1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / -10 °C / Inert atmosphere
3.1: sodium; methanol / 1 h / 0 - 20 °C / Inert atmosphere
4.1: pyridine / 72 h / 110 °C
5.1: potassium carbonate; palladium 10% on activated carbon; hydrogen / ethyl acetate / 48 h / 20 °C / 760.05 Torr
6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
7.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere
7.2: 0 - 20 °C / Inert atmosphere
With
pyridine; methanol; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; sodium; sodium hydride; diisobutylaluminium hydride; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; toluene; mineral oil;
2.1: |Mitsunobu Displacement / 7.2: |Williamson Ether Synthesis;
DOI:10.1055/s-0032-1317929
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium; methanol / 1 h / 0 - 20 °C / Inert atmosphere
2.1: pyridine / 72 h / 110 °C
3.1: potassium carbonate; palladium 10% on activated carbon; hydrogen / ethyl acetate / 48 h / 20 °C / 760.05 Torr
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere
5.2: 0 - 20 °C / Inert atmosphere
With
pyridine; methanol; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; sodium; sodium hydride; potassium carbonate;
In
tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
5.2: |Williamson Ether Synthesis;
DOI:10.1055/s-0032-1317929
