(2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone

Base Information

Chemical Name:(2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone
CAS No.:1258391-55-7
Molecular Formula:C₁₈H₁₆Br₂Cl₂O₅
Molecular Weight:543.036
Hs Code.:

Synonyms:(2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone

Suppliers and Price of (2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone

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Technology Process of (2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone

There total 1 articles about (2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1258391-53-5
(2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanol

: 1258391-55-7
(2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1002/anie.201003755

Reference yield: 97.0%

: 1258391-55-7
(2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone

: 1258391-68-2
(2,6-dibromo-3,5-dihydroxyphenyl)(3,5-dichloro-2-hydroxy-6-methoxy-4-methylphenyl)methanone

Guidance literature:: (2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone; With boron tribromide; In dichloromethane; at 0 - 20 ℃; for 3h; Inert atmosphere;

With water; In dichloromethane; Cooling with ice;
DOI:10.1002/anie.201003755

Reference yield: 87.0%

: 1258391-55-7
(2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone

: 870-63-3
prenyl bromide

: 1258391-57-9
(2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

Guidance literature:: (2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone; With phenyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

prenyl bromide; With copper(I) cyanide di(lithium chloride); In tetrahydrofuran; at 20 ℃; for 0.833333h;
DOI:10.1002/anie.201003755