(2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

Base Information

Chemical Name:(2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone
CAS No.:1258391-57-9
Molecular Formula:C₂₃H₂₅BrCl₂O₅
Molecular Weight:532.259
Hs Code.:

Synonyms:(2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

Suppliers and Price of (2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of (2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

There total 1 articles about (2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1258391-55-7
(2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone

: 870-63-3
prenyl bromide

: 1258391-57-9
(2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

Guidance literature:: (2,6-dibromo-3,5-dimethoxyphenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)-methanone; With phenyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

prenyl bromide; With copper(I) cyanide di(lithium chloride); In tetrahydrofuran; at 20 ℃; for 0.833333h;
DOI:10.1002/anie.201003755

Reference yield: 93.0%

: 1258391-57-9
(2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

: 1352630-71-7
C₂₀H₁₉BrCl₂O₄

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 0.75h;
DOI:10.1055/s-0030-1260320

Reference yield: 54.0%

: 1258391-57-9
(2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

: 109-94-4
formic acid ethyl ester

: 1258391-60-4
(2-formyl-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone

Guidance literature:: (2-bromo-3,5-dimethoxy-6-(3-methylbut-2-enyl)phenyl)(3,5-dichloro-2,6-dimethoxy-4-methylphenyl)methanone; With n-butyllithium; magnesium bromide ethyl etherate; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

formic acid ethyl ester; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1002/anie.201003755