Technology Process of C26H32O2
There total 5 articles about C26H32O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) n-butyllithium / 1.) THF, 1 h, 2.) 25 min
2: 36 percent / PBr3 / benzene / 2.5 h / 75 °C
3: 1.) ethylmagnesium bromide / 1.) THF, ether, reflux, 3 h, 2.) reflux
With
n-butyllithium; ethylmagnesium bromide; phosphorus tribromide;
In
benzene;
DOI:10.1021/jo00003a050
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 58 percent / Br2, AlCl3 / CH2Cl2 / 18 h / Ambient temperature
2: 56 percent / AlCl3 / benzene / 1 h / Ambient temperature
3: 1.) n-butyllithium / 1.) THF, 1 h, 2.) 25 min
4: 36 percent / PBr3 / benzene / 2.5 h / 75 °C
5: 1.) ethylmagnesium bromide / 1.) THF, ether, reflux, 3 h, 2.) reflux
With
n-butyllithium; aluminium trichloride; ethylmagnesium bromide; bromine; phosphorus tribromide;
In
dichloromethane; benzene;
DOI:10.1021/jo00003a050
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 56 percent / AlCl3 / benzene / 1 h / Ambient temperature
2: 1.) n-butyllithium / 1.) THF, 1 h, 2.) 25 min
3: 36 percent / PBr3 / benzene / 2.5 h / 75 °C
4: 1.) ethylmagnesium bromide / 1.) THF, ether, reflux, 3 h, 2.) reflux
With
n-butyllithium; aluminium trichloride; ethylmagnesium bromide; phosphorus tribromide;
In
benzene;
DOI:10.1021/jo00003a050
