(1S,3S)-2,2-Dimethyl-3-(3-methyl-2-oxo-butyl)-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Base Information

Chemical Name:(1S,3S)-2,2-Dimethyl-3-(3-methyl-2-oxo-butyl)-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester
CAS No.:120202-45-1
Molecular Formula:C₂₁H₃₆O₃
Molecular Weight:336.515
Hs Code.:

Synonyms:(1S,3S)-2,2-Dimethyl-3-(3-methyl-2-oxo-butyl)-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

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Chemical Property of (1S,3S)-2,2-Dimethyl-3-(3-methyl-2-oxo-butyl)-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

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Technology Process of (1S,3S)-2,2-Dimethyl-3-(3-methyl-2-oxo-butyl)-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

There total 3 articles about (1S,3S)-2,2-Dimethyl-3-(3-methyl-2-oxo-butyl)-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 120138-84-3,120202-46-2
(1S,3S)-3-{2-[1-Methoxycarbonyl-meth-(E)-ylidene]-3-methyl-butyl}-2,2-dimethyl-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 120202-45-1
(1S,3S)-2,2-Dimethyl-3-(3-methyl-2-oxo-butyl)-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: With ozone; In dichloromethane; at -78 ℃; for 0.5h;

Reference yield:

: 63254-50-2
L-menthyl diazoacetate

: 120202-45-1
(1S,3S)-2,2-Dimethyl-3-(3-methyl-2-oxo-butyl)-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 510 mg / CuL_C (L_C=chiral ligand with S configuration) / cyclohexane / 0.08 h / 80 °C

2: 91 percent / O₃ / CH₂Cl₂ / 0.5 h / -78 °C

With ozone; CuL_C (L_C=chiral ligand with S configuration); In dichloromethane; cyclohexane;

Reference yield:

: 80114-63-2
E-β-thujaketonic acid methyl ester

: 120202-45-1
(1S,3S)-2,2-Dimethyl-3-(3-methyl-2-oxo-butyl)-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 510 mg / CuL_C (L_C=chiral ligand with S configuration) / cyclohexane / 0.08 h / 80 °C

2: 91 percent / O₃ / CH₂Cl₂ / 0.5 h / -78 °C

With ozone; CuL_C (L_C=chiral ligand with S configuration); In dichloromethane; cyclohexane;