(1S,3S)-3-{2-[1-Methoxycarbonyl-meth-(E)-ylidene]-3-methyl-butyl}-2,2-dimethyl-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Base Information

• Chemical Name: (1S,3S)-3-{2-[1-Methoxycarbonyl-meth-(E)-ylidene]-3-methyl-butyl}-2,2-dimethyl-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester
• CAS No.: 120138-84-3
• Molecular Formula: C₂₄H₄₀O₄
• Molecular Weight: 392.579

Synonyms:

Chemical Property of (1S,3S)-3-{2-[1-Methoxycarbonyl-meth-(E)-ylidene]-3-methyl-butyl}-2,2-dimethyl-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Useful:

Technology Process of (1S,3S)-3-{2-[1-Methoxycarbonyl-meth-(E)-ylidene]-3-methyl-butyl}-2,2-dimethyl-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

There total 2 articles about (1S,3S)-3-{2-[1-Methoxycarbonyl-meth-(E)-ylidene]-3-methyl-butyl}-2,2-dimethyl-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-menthyl diazoacetate (63254-50-2) + E-β-thujaketonic acid methyl ester (80114-63-2) → (1R,3S)-3-{2-[1-Methoxycarbonyl-meth-(E)-ylidene]-3-methyl-butyl}-2,2-dimethyl-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (120138-84-3,120202-46-2) + (1S,3S)-3-{2-[1-Methoxycarbonyl-meth-(E)-ylidene]-3-methyl-butyl}-2,2-dimethyl-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (120138-84-3,120202-46-2)

Guidance literature:

CuL_C (L_C= chiral ligand with S configuration); In cyclohexane; at 80 ℃; for 0.0833333h;

Reference yield:

L-menthyl diazoacetate (63254-50-2) + E-β-thujaketonic acid methyl ester (80114-63-2) → (1R,3S)-3-{2-[1-Methoxycarbonyl-meth-(E)-ylidene]-3-methyl-butyl}-2,2-dimethyl-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (120138-84-3,120202-46-2) + (1S,3S)-3-{2-[1-Methoxycarbonyl-meth-(E)-ylidene]-3-methyl-butyl}-2,2-dimethyl-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (120138-84-3,120202-46-2)

Guidance literature:

CuL_C (L_C= chiral ligand with S configuration); In cyclohexane; at 80 ℃; for 0.0833333h;

Reference yield: 91.0%

(1S,3S)-3-{2-[1-Methoxycarbonyl-meth-(E)-ylidene]-3-methyl-butyl}-2,2-dimethyl-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (120138-84-3,120202-46-2) → (1S,3S)-2,2-Dimethyl-3-(3-methyl-2-oxo-butyl)-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester (120202-45-1)

Guidance literature:

With ozone; In dichloromethane; at -78 ℃; for 0.5h;

upstream raw materials:

L-menthyl diazoacetate

E-β-thujaketonic acid methyl ester

Downstream raw materials:

(1R,3S)-2,2-Dimethyl-3-(3-methyl-2-oxo-butyl)-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

(1S,3S)-2,2-Dimethyl-3-(3-methyl-2-oxo-butyl)-cyclopropanecarboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

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