C₁₅H₁₂BrNO

Base Information

• Chemical Name: C₁₅H₁₂BrNO
• CAS No.: 1192466-48-0
• Molecular Formula: C₁₅H₁₂BrNO
• Molecular Weight: 302.17
• Mol file: 1192466-48-0.mol

Synonyms:C₁₅H₁₂BrNO

Chemical Property of C₁₅H₁₂BrNO

Chemical Property:

Purity/Quality:

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Technology Process of C₁₅H₁₂BrNO

There total 1 articles about C₁₅H₁₂BrNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

m-bromobenzoic aldehyde (3132-99-8) + 2-aminoacetophenone (551-93-9) → C15H12BrNO (1192466-48-0)

Guidance literature:

With sodium hydroxide; In ethanol; at 0 - 20 ℃;

DOI:10.1021/acs.orglett.5b01654

Reference yield: 89.0%

C15H12BrNO (1192466-48-0) + 1-benzyl-3-diazo-1,3-dihydro-2H-indol-2-one (461677-71-4) → (E)-5-benzyl-6a-(3-bromostyryl)-5,6a-dihydro-6H-indolo[3,2-c]quinolin-6-one

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); In chloroform; at 60 ℃; for 16h;

DOI:10.1021/acs.orglett.8b03557

Reference yield: 87.0%

C15H12BrNO (1192466-48-0) → 2-(3-bromophenyl)-2,3-dihydroquinolin-4(1H)-one

Guidance literature:

With silica gel; ytterbium(III) triflate; at 80 ℃; for 3h; neat (no solvent);

DOI:10.3184/030823409X416974

upstream raw materials:

m-bromobenzoic aldehyde

2-aminoacetophenone

Downstream raw materials:

C₁₆H₁₁BrClNO