(2E)-3,6-anhydro-2-deoxy-2-C-(hydroxymethylidene)-4,5-O-isopropylidene-4-C-methyl-7-O-(triphenylmethyl)-D-allo-and D-altro-septononitrile

Base Information

Chemical Name:(2E)-3,6-anhydro-2-deoxy-2-C-(hydroxymethylidene)-4,5-O-isopropylidene-4-C-methyl-7-O-(triphenylmethyl)-D-allo-and D-altro-septononitrile
CAS No.:847551-32-0
Molecular Formula:C₃₁H₃₁NO₅
Molecular Weight:497.591
Hs Code.:

Synonyms:(2E)-3,6-anhydro-2-deoxy-2-C-(hydroxymethylidene)-4,5-O-isopropylidene-4-C-methyl-7-O-(triphenylmethyl)-D-allo-and D-altro-septononitrile

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Chemical Property of (2E)-3,6-anhydro-2-deoxy-2-C-(hydroxymethylidene)-4,5-O-isopropylidene-4-C-methyl-7-O-(triphenylmethyl)-D-allo-and D-altro-septononitrile

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Technology Process of (2E)-3,6-anhydro-2-deoxy-2-C-(hydroxymethylidene)-4,5-O-isopropylidene-4-C-methyl-7-O-(triphenylmethyl)-D-allo-and D-altro-septononitrile

There total 2 articles about (2E)-3,6-anhydro-2-deoxy-2-C-(hydroxymethylidene)-4,5-O-isopropylidene-4-C-methyl-7-O-(triphenylmethyl)-D-allo-and D-altro-septononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 847551-31-9
(2E)-3,6-anhydro-2-deoxy-2-C-[(N,N-dimethylamino)methylidene]-4,5-O-isopropylidene-4-C-methyl-7-O-(triphenylmethyl)-D-allo-and D-altro-septononitrile

: 847551-32-0
(2E)-3,6-anhydro-2-deoxy-2-C-(hydroxymethylidene)-4,5-O-isopropylidene-4-C-methyl-7-O-(triphenylmethyl)-D-allo-and D-altro-septononitrile

Guidance literature:: (2E)-3,6-anhydro-2-deoxy-2-C-[(N,N-dimethylamino)methylidene]-4,5-O-isopropylidene-4-C-methyl-7-O-(triphenylmethyl)-D-allo-and D-altro-septononitrile; With water; acetic acid; In tetrahydrofuran; for 1h;

With sodium hydrogencarbonate; In tetrahydrofuran; chloroform;

Reference yield:

: 107-31-3
Methyl formate

: 847551-32-0
(2E)-3,6-anhydro-2-deoxy-2-C-(hydroxymethylidene)-4,5-O-isopropylidene-4-C-methyl-7-O-(triphenylmethyl)-D-allo-and D-altro-septononitrile

Guidance literature:: 2-(2-C-methyl-2,3-O-(1-methylethylidene)-5-O-trityl-β-D-ribofuranosyl)acetonitrile; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.5h;

Methyl formate; In tetrahydrofuran; at -78 - 0 ℃; for 1.25h;