5-cyano-N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-((2-(dimethylamino)ethyl)(methyl)amino)-N-methylbenzenesulfonohydrazide hydrochloride

Base Information

Chemical Name:5-cyano-N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-((2-(dimethylamino)ethyl)(methyl)amino)-N-methylbenzenesulfonohydrazide hydrochloride
CAS No.:1101119-49-6
Molecular Formula:C₂₂H₂₄N₈O₂S*ClH
Molecular Weight:501.012
Hs Code.:

5-cyano-N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-((2-(dimethylamino)ethyl)(methyl)amino)-N-methylbenzenesulfonohydrazide hydrochloride

Synonyms:5-cyano-N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-((2-(dimethylamino)ethyl)(methyl)amino)-N-methylbenzenesulfonohydrazide hydrochloride

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Chemical Property of 5-cyano-N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-((2-(dimethylamino)ethyl)(methyl)amino)-N-methylbenzenesulfonohydrazide hydrochloride

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Technology Process of 5-cyano-N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-((2-(dimethylamino)ethyl)(methyl)amino)-N-methylbenzenesulfonohydrazide hydrochloride

There total 4 articles about 5-cyano-N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-((2-(dimethylamino)ethyl)(methyl)amino)-N-methylbenzenesulfonohydrazide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1101119-45-2
5-cyano-N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-fluoro-N-methylbenzenesulfonohydrazide

: 142-25-6
N,N',N'-trimethylenediamine

: 1101119-49-6
5-cyano-N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-((2-(dimethylamino)ethyl)(methyl)amino)-N-methylbenzenesulfonohydrazide hydrochloride

Guidance literature:: 5-cyano-N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-fluoro-N-methylbenzenesulfonohydrazide; N,N',N'-trimethylenediamine; In tetrahydrofuran; for 18h;

With hydrogenchloride; In methanol; dichloromethane; for 0.5h;
DOI:10.1016/j.bmcl.2016.11.078

Reference yield: 90.0%

: 1101119-49-6
5-cyano-N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-((2-(dimethylamino)ethyl)(methyl)amino)-N-methylbenzenesulfonohydrazide hydrochloride

Guidance literature:

Reference yield:

: 1101120-80-2
5-cyano-2-fluorobenzene-1-sulfonyl chloride

: 1101119-49-6
5-cyano-N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-((2-(dimethylamino)ethyl)(methyl)amino)-N-methylbenzenesulfonohydrazide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,6-dimethylpyridine / methanol / 0.5 h

2.1: tetrahydrofuran / 18 h

2.2: 0.5 h

With 2,6-dimethylpyridine; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2016.11.078