19α-methyl-(20α)-18-oxa-yohimb-16-ene-16-carboxylic acid methyl ester

Base Information

Chemical Name:19α-methyl-(20α)-18-oxa-yohimb-16-ene-16-carboxylic acid methyl ester
CAS No.:122441-12-7
Molecular Formula:C₂₁H₂₄N₂O₃
Molecular Weight:352.433
Hs Code.:

Synonyms:19α-methyl-(20α)-18-oxa-yohimb-16-ene-16-carboxylic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 19α-methyl-(20α)-18-oxa-yohimb-16-ene-16-carboxylic acid methyl ester

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Technology Process of 19α-methyl-(20α)-18-oxa-yohimb-16-ene-16-carboxylic acid methyl ester

There total 61 articles about 19α-methyl-(20α)-18-oxa-yohimb-16-ene-16-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: C₂₃H₂₆N₂O₆

: 483-03-4,483-04-5,642-17-1,5299-09-2,6474-90-4,6870-40-2,6884-17-9,20361-85-7,20361-86-8,24196-06-3,24196-08-5,24196-15-4,24196-16-5,25532-45-0,25532-46-1,112835-69-5,122441-12-7,132016-16-1
(+)-rauniticine

Guidance literature:: C₂₃H₂₆N₂O₆; With methanol; sodium tetrahydroborate; at -10 ℃; for 0.5h; Inert atmosphere;

With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 8h; Inert atmosphere; Reflux;

With methanol; potassium carbonate; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.chempr.2017.04.007

Reference yield:

: tryptamine hydrosuccinate

: secologanin

: 639-43-0,7344-80-1
akuammicine

: 483-03-4,483-04-5,642-17-1,5299-09-2,6474-90-4,6870-40-2,6884-17-9,20361-85-7,20361-86-8,24196-06-3,24196-08-5,24196-15-4,24196-16-5,25532-45-0,25532-46-1,112835-69-5,122441-12-7,132016-16-1
tetrahydroalstonine

: 2182-14-1
vindoline

Guidance literature:: With cell-free extracts from Catharanthus roseus; NADPH; flavin adenine dinucleotide; at 34 ℃; for 2h; Product distribution; Mechanism; biosynthesis of the products were studied; experiment was performed with <2-14C>tryptamine and the incorporation of the radiolabel into vindoline was investigated; different cell-free extracts;
DOI:10.1002/hlca.19820650716