(R)-Methyl-((S)-methylsulfanyl-phenyl-methyl)-naphthalen-1-yl-phenyl-silane

Base Information

Chemical Name:(R)-Methyl-((S)-methylsulfanyl-phenyl-methyl)-naphthalen-1-yl-phenyl-silane
CAS No.:115691-18-4
Molecular Formula:C₂₅H₂₄SSi
Molecular Weight:384.617
Hs Code.:

Synonyms:(R)-Methyl-((S)-methylsulfanyl-phenyl-methyl)-naphthalen-1-yl-phenyl-silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-Methyl-((S)-methylsulfanyl-phenyl-methyl)-naphthalen-1-yl-phenyl-silane

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Technology Process of (R)-Methyl-((S)-methylsulfanyl-phenyl-methyl)-naphthalen-1-yl-phenyl-silane

There total 3 articles about (R)-Methyl-((S)-methylsulfanyl-phenyl-methyl)-naphthalen-1-yl-phenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 917-54-4
methyllithium

: 115691-12-8
R-(-)-methyl-α-naphthyl-phenylsilyl phenyl thioketone

: 115691-14-0
(R)-Methyl-((R)-methylsulfanyl-phenyl-methyl)-naphthalen-1-yl-phenyl-silane

: 115691-18-4
(R)-Methyl-((S)-methylsulfanyl-phenyl-methyl)-naphthalen-1-yl-phenyl-silane

Guidance literature:: With methanol; In diethyl ether; at -80 ℃; Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(00)99096-8

Reference yield:

: 75-16-1
methylmagnesium bromide

: 115691-12-8
R-(-)-methyl-α-naphthyl-phenylsilyl phenyl thioketone

: 115691-14-0
(R)-Methyl-((R)-methylsulfanyl-phenyl-methyl)-naphthalen-1-yl-phenyl-silane

: 115691-18-4
(R)-Methyl-((S)-methylsulfanyl-phenyl-methyl)-naphthalen-1-yl-phenyl-silane

Guidance literature:: With methanol; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) Et₂O, -80 degC, 1h; 2.) -80 degC;
DOI:10.1016/S0040-4039(00)99096-8

Reference yield:

: 917-54-4
methyllithium

: 115691-12-8
R-(-)-methyl-α-naphthyl-phenylsilyl phenyl thioketone

: 115691-18-4
(R)-Methyl-((S)-methylsulfanyl-phenyl-methyl)-naphthalen-1-yl-phenyl-silane

Guidance literature:: With methyllithium; at -80 ℃; Product distribution; comparative studies with different solvents, quenching agents in different reaction time;
DOI:10.1016/S0040-4039(00)99096-8