3,6-di-tert-butyl-9-(3-(3,6-di-tert-butyl-9H-carbazol-9-yl)-9-tosyl-9H-carbazol-6-yl)-9H-carbazole

Base Information

Chemical Name:3,6-di-tert-butyl-9-(3-(3,6-di-tert-butyl-9H-carbazol-9-yl)-9-tosyl-9H-carbazol-6-yl)-9H-carbazole
CAS No.:551951-18-9
Molecular Formula:C₅₉H₆₁N₃O₂S
Molecular Weight:876.218
Hs Code.:

Synonyms:3,6-di-tert-butyl-9-(3-(3,6-di-tert-butyl-9H-carbazol-9-yl)-9-tosyl-9H-carbazol-6-yl)-9H-carbazole

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Chemical Property of 3,6-di-tert-butyl-9-(3-(3,6-di-tert-butyl-9H-carbazol-9-yl)-9-tosyl-9H-carbazol-6-yl)-9H-carbazole

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Technology Process of 3,6-di-tert-butyl-9-(3-(3,6-di-tert-butyl-9H-carbazol-9-yl)-9-tosyl-9H-carbazol-6-yl)-9H-carbazole

There total 8 articles about 3,6-di-tert-butyl-9-(3-(3,6-di-tert-butyl-9H-carbazol-9-yl)-9-tosyl-9H-carbazol-6-yl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 37500-95-1
3,6-di(tert-butyl)-9H-carbazole

: 551951-03-2
3,6-diiodo-9-(4-toluenesulfonyl)-9H-carbazole

: 551951-18-9
3,6-di-tert-butyl-9-(3-(3,6-di-tert-butyl-9H-carbazol-9-yl)-9-tosyl-9H-carbazol-6-yl)-9H-carbazole

Guidance literature:: With copper(l) iodide; K₃PO₄; trans-1,2-Diaminocyclohexane; In toluene; at 110 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c2cc16878b

Reference yield:

: 57103-02-3
3,6-diiodocarbazole

: 551951-18-9
3,6-di-tert-butyl-9-(3-(3,6-di-tert-butyl-9H-carbazol-9-yl)-9-tosyl-9H-carbazol-6-yl)-9H-carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / 20 °C / Inert atmosphere

2: copper peroxide / 150 °C / Inert atmosphere

With copper peroxide; sodium hydride;
DOI:10.1039/c0dt01559h

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 551951-18-9
3,6-di-tert-butyl-9-(3-(3,6-di-tert-butyl-9H-carbazol-9-yl)-9-tosyl-9H-carbazol-6-yl)-9H-carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

2: copper peroxide / 150 °C / Inert atmosphere

With aluminum (III) chloride; copper peroxide; In dichloromethane;
DOI:10.1039/c0dt01559h