N,N-bis(2-hydroxyethyl)-4-<5-pentanamido>aniline

Base Information

Chemical Name:N,N-bis(2-hydroxyethyl)-4-<5-pentanamido>aniline
CAS No.:125174-08-5
Molecular Formula:C₂₃H₃₁N₃O₅
Molecular Weight:429.516
Hs Code.:

N,N-bis(2-hydroxyethyl)-4-<5-<N-(benzyloxycarbonyl)amino>pentanamido>aniline

Synonyms:N,N-bis(2-hydroxyethyl)-4-<5-pentanamido>aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-bis(2-hydroxyethyl)-4-<5-pentanamido>aniline

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Technology Process of N,N-bis(2-hydroxyethyl)-4-<5-pentanamido>aniline

There total 1 articles about N,N-bis(2-hydroxyethyl)-4-<5-pentanamido>aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23135-50-4
5-(N-benzyloxycarbonylamino)pentanoic acid

: 7575-35-1
N,N-bis(2-hydroxyethyl)-4-aminoaniline

: 125174-08-5
N,N-bis(2-hydroxyethyl)-4-<5-pentanamido>aniline

Guidance literature:: With 1,1'-carbonyldiimidazole; Yield given. Multistep reaction; 1.) DMF, 40 deg C, 30 min, 2.) 20 deg C, 10 h;
DOI:10.1021/jm00166a015

Reference yield: 25.0%

: 125174-08-5
N,N-bis(2-hydroxyethyl)-4-<5-pentanamido>aniline

: 125174-09-6
N,N-bis(2-chloroethyl)-4-<5-pentanamido>aniline

Guidance literature:: With thionyl chloride; In 1,2-dichloro-ethane; for 0.5h; Heating;
DOI:10.1021/jm00166a015

Reference yield:

: 125174-08-5
N,N-bis(2-hydroxyethyl)-4-<5-pentanamido>aniline

: 125174-10-9
5-Amino-pentanoic acid {4-[bis-(2-chloro-ethyl)-amino]-phenyl}-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 25 percent / SOCl₂ / 1,2-dichloro-ethane / 0.5 h / Heating

2: HBr/AcOH / 4 h / 20 °C

With thionyl chloride; hydrogen bromide; acetic acid; In 1,2-dichloro-ethane;
DOI:10.1021/jm00166a015