ethyl 4-(pyridin-4-ylmethyl)benzoate

Base Information

Chemical Name:ethyl 4-(pyridin-4-ylmethyl)benzoate
CAS No.:1334723-70-4
Molecular Formula:C₁₅H₁₅NO₂
Molecular Weight:241.29
Hs Code.:

Synonyms:ethyl 4-(pyridin-4-ylmethyl)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 4-(pyridin-4-ylmethyl)benzoate

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Technology Process of ethyl 4-(pyridin-4-ylmethyl)benzoate

There total 1 articles about ethyl 4-(pyridin-4-ylmethyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 108-89-4
picoline

: 5798-75-4
Ethyl 4-bromobenzoate

: 1334723-70-4
ethyl 4-(pyridin-4-ylmethyl)benzoate

Guidance literature:: picoline; With zinc chloride-2,2,6,6-tetramethylpiperidin-1-ide lithium chloride complex; In tetrahydrofuran; at 25 ℃; for 1h; Inert atmosphere;

With scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; at 25 ℃; for 0.25h; Inert atmosphere;

Ethyl 4-bromobenzoate; With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; In tetrahydrofuran; at 50 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201103074

Reference yield: 61.0%

: 1334723-70-4
ethyl 4-(pyridin-4-ylmethyl)benzoate

: ethyl 4-(pyridin-4-ylcarbonyl)benzoate

Guidance literature:: With iron(II) chloride tetrahydrate; oxygen; acetic acid; In dimethyl sulfoxide; at 100 ℃; for 24h; under 760.051 Torr;
DOI:10.3762/bjoc.12.16