4-<<(Ethoxycarbonyl)methyl>imino>-5-hydroxy-1-methyl-5-phenyl-3-isopropyl-2-thioxo-1,3-diazolidine

Base Information

Chemical Name:4-<<(Ethoxycarbonyl)methyl>imino>-5-hydroxy-1-methyl-5-phenyl-3-isopropyl-2-thioxo-1,3-diazolidine
CAS No.:138877-79-9
Molecular Formula:C₁₇H₂₃N₃O₃S
Molecular Weight:349.454
Hs Code.:

Synonyms:4-<<(Ethoxycarbonyl)methyl>imino>-5-hydroxy-1-methyl-5-phenyl-3-isopropyl-2-thioxo-1,3-diazolidine

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Chemical Property of 4-<<(Ethoxycarbonyl)methyl>imino>-5-hydroxy-1-methyl-5-phenyl-3-isopropyl-2-thioxo-1,3-diazolidine

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Technology Process of 4-<<(Ethoxycarbonyl)methyl>imino>-5-hydroxy-1-methyl-5-phenyl-3-isopropyl-2-thioxo-1,3-diazolidine

There total 3 articles about 4-<<(Ethoxycarbonyl)methyl>imino>-5-hydroxy-1-methyl-5-phenyl-3-isopropyl-2-thioxo-1,3-diazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 138877-69-7
4-<<(Ethoxycarbonyl)methyl>amino>-1-methyl-2-(methylthio)-5-phenyl-3-isopropylimidazolium chloride

: 138877-79-9
4-<<(Ethoxycarbonyl)methyl>imino>-5-hydroxy-1-methyl-5-phenyl-3-isopropyl-2-thioxo-1,3-diazolidine

Guidance literature:: With air; In toluene; for 1h; Heating;
DOI:10.1021/jo00033a038

Reference yield:

: 2999-46-4
Ethyl isocyanoacetate

: 138877-79-9
4-<<(Ethoxycarbonyl)methyl>imino>-5-hydroxy-1-methyl-5-phenyl-3-isopropyl-2-thioxo-1,3-diazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / CHCl₃ / 65 h / 20 °C

2: 65 percent / air / toluene / 1 h / Heating

With air; In chloroform; toluene;
DOI:10.1021/jo00033a038

Reference yield:

: 622-29-7
N-Benzylidenemethylamine

: 138877-79-9
4-<<(Ethoxycarbonyl)methyl>imino>-5-hydroxy-1-methyl-5-phenyl-3-isopropyl-2-thioxo-1,3-diazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / CHCl₃ / 65 h / 20 °C

2: 65 percent / air / toluene / 1 h / Heating

With air; In chloroform; toluene;
DOI:10.1021/jo00033a038