O,O'-di-tert-butyl 4-methyl-1,3-phenylenedicarbamate

Base Information

Chemical Name:O,O'-di-tert-butyl 4-methyl-1,3-phenylenedicarbamate
CAS No.:59255-79-7
Molecular Formula:C₁₇H₂₆N₂O₄
Molecular Weight:322.404
Hs Code.:

Synonyms:O,O'-di-tert-butyl 4-methyl-1,3-phenylenedicarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O,O'-di-tert-butyl 4-methyl-1,3-phenylenedicarbamate

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Technology Process of O,O'-di-tert-butyl 4-methyl-1,3-phenylenedicarbamate

There total 2 articles about O,O'-di-tert-butyl 4-methyl-1,3-phenylenedicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 584-84-9,6144-18-9,26006-20-2
2,4-Toluene diisocyanate

: 75-65-0
tert-butyl alcohol

: 59255-79-7
O,O'-di-tert-butyl 4-methyl-1,3-phenylenedicarbamate

Guidance literature:: tert-butyl alcohol; With dibutyltin dilaurate; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere;

2,4-Toluene diisocyanate; In N,N-dimethyl-formamide; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1002/anie.201800795